Beer decolorizing film and preparation method thereof
A beer and decolorization technology, applied in the preparation of alcoholic beverages, chemical instruments and methods, membrane technology, etc., can solve problems such as high operating pressure requirements, consumables, solid-liquid separation, etc., to improve swelling resistance, improve osmotic flow Quantity, strong anti-pollution effect
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Embodiment 1
[0033] Embodiment 1 (comparative example)
[0034] Dissolve PVA powder in hot water at 85°C to prepare a 5% PVA solution; dissolve PAA powder in hot water at 90°C to prepare a 1% PAA solution; mix the above two solutions at a ratio of 1:1, Stir for 24 hours until uniformly mixed to obtain a hydrophilic coating solution. PEI, NMP and LiCl were formulated into a base film liquid at a weight ratio of 12:60:28, coated on the surface of a non-woven fabric, and then immersed in deionized water at 25°C to prepare a base film. The hydrophilic coating solution is applied by slit extrusion coating method, the solution extrusion rate is 0.8mL / min, coated on the surface of the PEI base film, and placed in an oven at 130°C for interfacial polymerization reaction for 4 hours to obtain a non-blocking solution And the PVA / PAA / PEI beer decolorization composite film prepared by the method without cross-linking agent.
Embodiment 2
[0035] Embodiment 2 (comparative example)
[0036] Dissolve PVA powder in hot water at 90°C to prepare a 7% PVA solution; dissolve PAA powder in hot water at 90°C to prepare a 2% PAA solution; mix the above two solutions at a ratio of 1:3, Stir for 24 hours until uniformly mixed to obtain a hydrophilic coating solution. PEI, NMP and LiCl were formulated into a base film liquid at a weight ratio of 15:65:20, coated on the surface of a non-woven fabric, and then immersed in deionized water at 25°C to prepare a base film. The hydrophilic coating solution is applied by slit extrusion coating method, the solution extrusion rate is 1mL / min, coated on the surface of the PEI base film, and placed in an oven at 140°C for interfacial polymerization reaction for 6 hours to obtain a non-blocking solution and PVA / PAA / PEI beer decolorization composite film prepared by cross-linking agent-free method.
Embodiment 3
[0037] Embodiment 3 (comparative example)
[0038] Dissolve PVA powder in 95°C hot water to prepare 8% PVA solution; dissolve PAA powder in 90°C hot water to prepare 3% PAA solution; mix the above two solutions in a ratio of 1:5, Stir for 24 hours until uniformly mixed to obtain a hydrophilic coating solution. PEI, NMP and LiCl were formulated into a base film solution at a weight ratio of 20:70:10, coated on the surface of a non-woven fabric, and then immersed in deionized water at 25°C to prepare a base film. The hydrophilic coating solution is applied by slit extrusion coating method, the solution extrusion rate is 1.5mL / min, coated on the surface of the PEI base film, placed in an oven at 150°C for interfacial polymerization reaction for 8 hours, and a non-blocking solution is obtained And the PVA / PAA / PEI beer decolorization composite film prepared by the method without cross-linking agent.
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