Temporary plugging agent assisted carbon dioxide huff and puff oil extraction method
A technology of carbon dioxide and temporary plugging agent, applied in chemical instruments and methods, production fluids, earthwork drilling, etc., can solve the problems of poor sealing performance, long plugging validity period, and reduced plugging ability of dominant seepage channels in reservoirs. It is beneficial to the recovery of reservoir permeability, has a wide range of applications, and improves the plugging strength.
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Embodiment 1
[0041] Embodiment 1: the preparation of temporary plugging agent
[0042] In the present invention, 50 g of deionized water and 10 g of acrylic acid are added to a 500 ml round bottom flask, the pH value is adjusted to 7 to 7.5 with sodium hydroxide, and then 16 g of acrylamide, 0.15 g of allyl sodium sulfonate, and 0.03 g of dipropylene glycol diacrylic acid are added. After fully stirring, add a certain amount of deionized water to form a solution with a mass concentration of 30%, and ventilate nitrogen to remove oxygen; add 0.07g ammonium persulfate-sodium bisulfite initiator, stir to dissolve it, and obtain the obtained The temporary blocking agent.
Embodiment 2
[0043] Embodiment 2: Polymerization of temporary plugging agent
[0044] Seal the temporary blocking agent obtained in Example 1 and place it in a thermostat at 60°C, take it out after 24 hours, dry it and pulverize it to obtain the polymerization product of the temporary blocking agent.
Embodiment 3
[0045] Embodiment 3: Characterization of temporary plugging agent polymerization product
[0046] The infrared spectrogram of the temporary plugging agent polymerization product of embodiment 2 gained is as follows figure 2 As shown, the N-H stretching vibration absorption peak is located at 3434cm -1 ; C-H stretching vibration absorption peak in methylene is located at 2927cm -1 ; The C-H antisymmetric stretching vibration absorption peak in the methyl group is located at 2855cm -1 ;C=O stretching vibration absorption peak is located at 1629cm -1 ; The C-H in-plane bending vibration absorption peak in the methyl group is located at 1460cm -1 ; The C-N stretching vibration absorption peak in the primary amide is located at 1407cm -1 ; The C-O stretching vibration absorption peak of the carboxyl group is located at 1325cm -1 ; C-O-C stretching vibration absorption peak in dipropylene glycol diacrylate is located at 1176cm -1 ; Primary amides -NH 2 The in-plane rocking v...
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