Preparation method of hydrogel cooling cloth

A technology of hydrogel cooling cloth and chloroform, which is applied in the fields of dyeing, textiles and papermaking, can solve the problems of poor air permeability and affecting the thermal and physiological comfort of the human body, so as to reduce the vapor pressure, accelerate the evaporation of water, and reduce the temperature of the human body. The effect of temperature

Pending Publication Date: 2022-02-15
国佳凝胶科创中心(深圳)有限公司
View PDF5 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In summer, when the sun shines strongly, people will sweat a lot outdoors due to the high ambient temperature. The sweat will soak through the clothing fabric and adhere to the surface of the skin. The air permeability is poor, which greatly affects the thermal physiological comfort of the human body.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] Follow the steps below to prepare the hydrogel cleaves:

[0027] S1. Elderly oxygen-based cage sedamine oxide, aluminum tetrachloride is added to trichloromethane, stirring is mixed with uniform nitrogen gas protection to add diethylamine, heating to the reflux temperature, heat after stirring, 4.5 hours to obtain reactants The reactant was filtered to remove the reactant to obtain a filter residue, and the filter residue was washed 3 times with trichloromethane and distilled water, and dried into a vacuum oven at 50 ° C to a constant weight to be modified by modified POSS spare, octal epoxy formation The ratio of siloxane, aluminum tetrachloride, trichloromethane, diethylamine is 1 mmol: 0.01 mmol: 18 ml: 1 mmol;

[0028] S2. In the proportion of 1 g: 1.5 g: 6 mL, the Poss S1 is modified, and the pH is added to trichloromethane, and the pH is adjusted to 2% by weight of 10%, and the pH is adjusted to 85 ° C after holding the stirring reaction. 9 hours, the pH value of 8 wa...

Embodiment 2

[0034] S1. Elderly oxygen-based cage sediment semisoxane, aluminum tetrachloride is added to trichloromethane, and the addition of diethylamine under uniform nitrogen gas protection is added, and the heat is stirred after the reflux temperature for 4 hours to obtain reactants. The reactant was filtered to remove the reactant to obtain a filter residue, and the filter residue was washed 3 times with trichloromethane and distilled water, and dried into a vacuum oven at 50 ° C to a constant weight to be modified by modified POSS spare, octal epoxy formation The ratio of siloxane, aluminum tetrachloride, trichloromethane, diethylamine is 1 mmol: 0.01 mmol: 18 ml: 1 mmol;

[0035] S2. In the proportion of 1 g: 1.5 g: 6 mL, the Poss S1 is modified, and the pH is added to trichloromethane, and the pH is adjusted to 2% by weight of 10%, and the pH is adjusted to 85 ° C after holding the stirring reaction. 10 hours, the pH value of 8 was adjusted with a hydroxide solution having a mass con...

Embodiment 3

[0041] S1. Eight epoxy cage silsesquioxane, aluminum trichloride was added chloroform, stir through diethylamine under nitrogen, was heated to reflux temperature after the incubation the reaction was stirred for 4.2 hours to obtain a reaction product the reaction residue was suction-filtered under reduced pressure, the residue was washed with chloroform 3 times and distilled water, respectively, into a vacuum oven at 50 deg.] C and dried to constant weight to give the standby POSS modified, epoxy eight cage silsesquioxane the proportion of silicone, aluminum chloride, chloroform, diethylamine is 1mmol: 0.01mmol: 18mL: 1mmol;

[0042] S2 to 1g:. 1.5g: 6mL ratio obtained in step S1 of the POSS modified, peppermint oil added chloroform, the mass concentration of 10% diluted hydrochloric acid to adjust the pH 2, heated to 85 ℃ incubation the reaction was stirred 8.5 hours, with a concentration of 10 mass% sodium hydroxide solution to adjust the pH to 8, to obtain a reaction solution a...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention provides a preparation method of hydrogel cooling cloth. The preparation method comprises the following steps: S1, carrying out reaction on octa-epoxy polyhedral oligomeric silsesquioxane, aluminum trichloride, trichloromethane and diethylamine to obtain modified POSS; S2, enabling reaction of the modified POSS obtained in the step S1, peppermint oil and trichloromethane to obtain a peppermint oil compound; S3, enabling reaction of sodium polyacrylate, carboxymethyl cellulose, montmorillonite, deionized water, malic acid and aluminum hydroxide to obtain hydrogel powder; S4, uniformly mixing the hydrogel powder obtained in the step S3, a microcapsule phase change material and the peppermint oil compound obtained in the step S2 to obtain a hydrogel cooling component for later use; S5, uniformly mixing the hydrogel cooling component obtained in the step S4, an adhesive, a thickening agent and a solvent to obtain printing paste for later use; and S6, printing the printing paste obtained in the step S5 on cloth, and transferring the cloth into a vacuum oven for drying to obtain the hydrogel cooling cloth. The hydrogel cooling cloth prepared by the invention can reduce the temperature of a human body, so that the human body is dry and comfortable.

Description

Technical field [0001] The present invention relates to a method of preparing a hydrogel clear cloth. Background technique [0002] With the improvement of living standards, people have higher requirements for clothing fabrics, and comfort is one of the main needs. Among them, people have great demand for the cool and comfortable functions of summer clothing, hoping that the body temperature can be kept in a comfortable time during outdoor activities. Summer sun is strongly illuminated, people will be excessive in the living temperature, the body is sweating, and the sweat will soake the clothing cloth, adhere to the skin surface, the gas permeability, greatly affect the thermophysical comfort of the human body. Inventive content [0003] The technical problem to be solved by the present invention is to provide a preparation method of hydrogel cleaning cloth, which is made of hydrogel cooling to reduce the human body, so that the human body is dry and comfortable. [0004] In or...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/52D06P1/50D06P1/44D06P1/651D06P1/653D06P1/673
CPCD06P1/5292D06P1/445D06P1/5257D06P1/50D06P1/67383D06P1/6735D06P1/6533D06P1/65162
Inventor 王梦纯
Owner 国佳凝胶科创中心(深圳)有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap