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Preparation method of deodorizing far-infrared health-care regenerated cellulose fiber

A far-infrared health care and regenerated cellulose technology, applied in the field of fibers, can solve the problems of large loss, loss, and lack of protection, and achieve the effect of durable deodorization, promoting blood circulation, and activating cells and tissues.

Pending Publication Date: 2022-02-15
潍坊欣龙生物材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Moreover, the solid substances added are easy to lose without protection treatment, and the functionality and durability of the product cannot be guaranteed.
Invention patent CN103556275B A far-infrared bamboo charcoal viscose fiber and its preparation method. The far-infrared ceramic powder added in this patent technology is composed of metal or metal oxide, which is very prone to sedimentation, and both bamboo charcoal powder and far-infrared ceramic powder are solid , the adsorption capacity of bamboo charcoal is very limited, which seriously affects the physical and mechanical properties and spinnability of fibers, thus affecting the functionality of fibers or fabrics.
[0004] Invention patent CN109943901A discloses deodorizing fiber and its manufacturing method. It is a kind of fiber masterbatch that is added to nylon with zeolite powder and lauric acid. It is melt-spun at a maximum temperature of 280°C, and the lauric acid component is lost at a higher temperature. More seriously, the prepared deodorant fiber has unsatisfactory functionality, and the fiber is a synthetic fiber, and the product is difficult to degrade naturally
However, the spinning and forming process of cellulose fibers is a strong acid system. If the deodorant is directly added to the spinning solution without protection treatment, the loss will be large, and the ideal deodorizing effect cannot be achieved.

Method used

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  • Preparation method of deodorizing far-infrared health-care regenerated cellulose fiber

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] 1. Preparation of mixed slurry

[0029] Under continuous stirring, slowly add bamboo charcoal powder and deodorant into deionized water in turn, after stirring for 30 minutes, add dispersant sodium hexametaphosphate and nanocellulose, grind and disperse for 30 minutes with a sand mill, and detect the particle size of the slurry The D90 is 1.676 μm, and a mixed slurry with a mass fraction of 20% is made.

[0030] The added amount of the dispersant is 0.5wt% (relative to the weight of the dispersion), the mass ratio of sodium hexametaphosphate to nanocellulose is 1:1, and the mass ratio of bamboo charcoal to deodorant in the mixed slurry is 2:1.

[0031] The model of the deodorant is JYKZOT-92.

[0032] 2. Preparation of blended spinning solution

[0033] Using cellulose pulp as raw material, the cellulose spinning stock solution was obtained through the conventional viscose preparation process. Its composition: 9.65% of cellulose A, 5.30% of sodium hydroxide, and falli...

Embodiment 2

[0040] 1. Preparation of mixed slurry

[0041] Under continuous stirring, slowly add bamboo charcoal powder and deodorant into deionized water in turn, after stirring for 30 minutes, add dispersant sodium hexametaphosphate and animal gelatin, grind and disperse with a sand mill for 45 minutes, and measure the particle size D90 of the slurry is 1.842 μm, and a slurry with a mass fraction of 25% is made.

[0042] The added amount of the dispersant is 1.5wt% (to the weight of the dispersion liquid), the mass ratio of sodium hexametaphosphate and animal gelatin is 1:1, and the mass ratio of bamboo charcoal and deodorant in the mixed slurry is 2:1.

[0043] The model of the deodorant is JYKZOT-92.

[0044] 2. Preparation of blended spinning solution

[0045] Using cellulose pulp as raw material, the cellulose spinning stock solution was obtained through the conventional viscose preparation process. Its composition: 10.3% of cellulose A, 6.0% of sodium hydroxide, and falling ball ...

Embodiment 3

[0052] 1. Preparation of bamboo charcoal slurry

[0053] Under continuous stirring, slowly add bamboo charcoal powder and deodorant into deionized water in turn, after stirring for 30 minutes, add dispersant sodium tripolyphosphate and nanocellulose, grind and disperse with a sand mill for 60 minutes, and detect the particle size of the slurry The D90 is 1.765 μm, and a slurry with a mass fraction of bamboo charcoal powder of 35% is made.

[0054] The added amount of the dispersant is 2.0wt% (to the weight of the dispersion liquid), the mass ratio of sodium tripolyphosphate and nanocellulose is 1:1, and the mass ratio of bamboo charcoal and deodorant in the mixed slurry is 2:1.

[0055] The model of the deodorant is JYKZOT-92.

[0056] 2. Preparation of blended spinning solution

[0057] Using cellulose pulp as raw material, the cellulose spinning stock solution is obtained through the conventional viscose preparation process. Its composition is: 10.8% of cellulose A, 6.4% o...

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Abstract

The invention provides a preparation method of a deodorizing far-infrared health-care regenerated cellulose fiber, and the preparation method comprises the following steps: preparing a mixed slurry, preparing a blended spinning solution, spinning, and deodorizing and finishing. According to the deodorizing far-infrared health-care regenerated cellulose fiber prepared by the method, the dry breaking strength is larger than or equal to 2.30 cN / dtex, the wet breaking strength is larger than or equal to 1.1 cN / dtex, the dry breaking elongation is larger than or equal to 18.0%, the 2-nonenal elimination rate is larger than or equal to 90%, the deodorizing far-infrared health-care regenerated cellulose fiber has a remarkable deodorizing function, the far-infrared normal emissivity is larger than or equal to 0.80, and the deodorizing far-infrared health-care regenerated cellulose fiber has the health-care functions of activating cell tissues and promoting blood circulation.

Description

technical field [0001] The invention relates to a regenerated cellulose fiber and a preparation method thereof, in particular to a regenerated cellulose fiber with deodorizing and far-infrared health care functions and a preparation method thereof, belonging to the field of fiber technology. Background technique [0002] With the continuous progress of my country's economy and social civilization, the requirements of the broad masses of the people for life taste and social environment are also increasing. After middle age, body functions begin to decline slowly, and the oxidation rate of the skin will also accelerate. In addition to prone to age spots, the oxidation of the skin will also produce a substance called 2-nonenal. At the same time, there will be the oil secreted on the skin or the smell of some bacteria, which will produce a smell, which is commonly called the smell of the elderly or the smell of the old. Hygiene and health care have become the focus of people's ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F2/10D01F1/10D01F11/02
CPCD01F2/10D01F1/10D01F11/02
Inventor 李昌垒刘乐孙东升秦翠梅马君志王东房德建李利建
Owner 潍坊欣龙生物材料有限公司
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