Preparation process of dimethyl carbonate and catalyst thereof
A technology for the preparation of dimethyl carbonate and its preparation process, which is applied in the field of the preparation process of dimethyl carbonate and its catalyst, and can solve the problems of high catalyst preparation cost and unsatisfactory conversion rate of catalyst to methanol, etc.
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Embodiment 1
[0029] A kind of preparation technology of dimethyl carbonate, comprises the steps:
[0030] (1) Grind the sulfuric acid slag after drying at 50°C for 1 hour, pass through a 100-mesh sieve, and the sieve residue is less than 1.5%. Mix the obtained sulfuric acid slag with a sulfuric acid solution with a mass fraction of 10%, and add the sulfuric acid solution according to the ratio of 1g:1.5ml of sulfuric acid in the sulfuric acid slag and sulfuric acid solution, the temperature of the acid leaching treatment is 55°C, and the time is 105min , after completion, filter for solid-liquid separation to obtain pretreated sulfuric acid slag for future use.
[0031] (2) The sulfuric acid slag of described pretreatment is mixed with the sulfuric acid of mass fraction 35%, and the ratio of sulfuric acid slag and sulfuric acid is 1g: 3ml, and the temperature of described acid leaching treatment is 55 ℃, and the time is 180min, after finishing, filter and solidify Liquid separation, washi...
Embodiment 2
[0038] A kind of preparation technology of dimethyl carbonate, comprises the steps:
[0039] (1) Grind the sulfuric acid slag after drying at 50°C for 1 hour, pass through a 100-mesh sieve, and the sieve residue is less than 1.5%. Mix the obtained sulfuric acid slag with a sulfuric acid solution with a mass fraction of 5%, and add the sulfuric acid solution according to the ratio of sulfuric acid slag and sulfuric acid in the sulfuric acid solution: 1g: 1.7ml, the temperature of the acid leaching treatment is 65°C, and the time is 90min , after completion, filter for solid-liquid separation to obtain pretreated sulfuric acid slag for future use.
[0040] (2) The sulfuric acid slag of described pretreatment is mixed with the sulfuric acid of mass fraction 30%, and the ratio of sulfuric acid slag and sulfuric acid is 1g: 4ml, and the temperature of described acid leaching treatment is 65 ℃, and the time is 100min, after completion, filter and solidify Liquid-liquid separation, ...
Embodiment 3
[0047] A kind of preparation technology of dimethyl carbonate, comprises the steps:
[0048] (1) Grind the sulfuric acid slag after drying at 50°C for 1 hour, pass through a 90-mesh sieve, and the sieve residue is less than 1.5%. Mix the obtained sulfuric acid slag with a sulfuric acid solution with a mass fraction of 15%, and add the sulfuric acid solution according to the ratio of 1g:1.4ml of sulfuric acid in the sulfuric acid slag and sulfuric acid solution. The temperature of the acid leaching treatment is 40°C and the time is 120min , after completion, filter for solid-liquid separation to obtain pretreated sulfuric acid slag for future use.
[0049] (2) The sulfuric acid slag of described pretreatment is mixed with the sulfuric acid of mass fraction 45%, and the ratio of sulfuric acid slag and sulfuric acid is 1g: 2.5ml, and the temperature of described acid leaching treatment is 40 ℃, and the time is 240min, after finishing, filter and carry out Separation of solid and...
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