Organic silicon complete variable-pressure thermal coupling rectification device and rectification method
A technology of thermal coupling and organic silicon, which is applied in the field of organic silicon rectification, can solve the problems of increasing equipment investment, affecting the smooth operation of the system, and not solving the problem of energy consumption of the de-higher tower, so as to achieve the effect of reducing equipment investment
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Embodiment 1
[0068] Such as figure 1 The shown organosilicon complete pressure-swing thermally coupled rectification device includes: de-higher tower 1, lower-lower tower 2, high-pressure binary tower 3 and low-pressure binary tower 4,
[0069] The tower kettle of the lowering tower 1 is provided with a coupling reboiler 12 for taking off the lowering tower tower kettle, and the tower kettle of the low-pressure binary tower 4 is provided with a low-pressure binary tower tower kettle coupling reboiler 13;
[0070]The tower top of the height-removing tower 1 is connected with the coupling reboiler 13 of the low-pressure binary tower still, and the gas phase stream at the top of the height-removing tower 1 provides a heat source for the low-pressure binary tower still, and the gas phase flowing out of the tower top of the height-removing tower 1 The stream enters the shell-side inlet of the low-pressure binary column column coupling reboiler 13, and the shell-side outlet of the low-pressure b...
Embodiment 2
[0080] use as figure 1 The rectification unit shown is used for the separation of crude methylchlorosilane monomer. The feed rate of the methyl chlorosilane crude monomer is 25000kg / hr, wherein in terms of mass fraction: Me1 is 60%, Me2 is 82%, Me3 is 5.6%, and the rest are high boilers and low boilers. The crude methyl chlorosilane monomer enters the de-altitude tower, and the heavy components are extracted from the bottom of the tower, including part of dimethyl dichlorosilane and high boilers with a higher boiling point than dimethyl dichlorosilane; dimethyl dichlorosilane is extracted from the top of the tower. Chlorosilane and light components with a lower boiling point than dimethyldichlorosilane, the top extract is used as the heat source of the low-pressure binary column coupling reboiler, and is cooled after exchanging heat with the column liquid in the coupled reboiler , and then enter the lowering tower. The top extraction of the lowering tower includes trimethylm...
Embodiment 3
[0090] The raw material conditions are as follows: the feed rate of the crude methyl chlorosilane monomer is 25000kg / hr, wherein in terms of mass fraction: Me1 is 5%, Me2 is 83%, Me3 is 5.6%, and the rest are high boilers and low boilers . All the other conditions are the same as in Example 2. The material recovery of each tower is shown in Table 3.
[0091] Table 3 The material recovery situation of each tower
[0092]
[0093]
[0094] Under the same processing capacity and product requirements, the comparison data of energy consumption between the non-coupling process and the coupled process in Example 3 are shown in Table 4.
[0095] Table 4 Energy Consumption Comparison of Coupling Process and Non-Coupling Process in Example 3
[0096]
[0097] From the comparative data shown in Table 4, it can be seen that the load of the reboiler is only 53% of that of the non-coupling process, and the load of the condenser is only 50% of the coupling process, so that the c...
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