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Light-resistant graphene UV ink and preparation method thereof

A graphene and ink technology, applied in inks, household appliances, applications, etc., can solve the problems of affecting the appearance and service life of the film material, easy to generate static electricity, fading and other problems, and achieve a long product validity period, a large light response range, and a preparation process. simple effect

Inactive Publication Date: 2021-12-07
南通吉美装饰材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, resins and pigments in UV inks are easily affected by light, temperature and humidity, causing fading and discoloration, which makes PVC decorative panels age after a period of use. In addition, due to the poor hydrophilicity of PVC, it is easy to Generate static electricity, which affects the appearance and service life of the membrane material, seriously restricting the development of PVC membrane material

Method used

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  • Light-resistant graphene UV ink and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] 1. Preparation of light-resistant graphene UV ink

[0033] (1) Raw material ratio is as follows (mass fraction):

[0034] Urethane Acrylic 42%

[0035] Photocatalytic modified graphene 4.0%

[0036] Zinc Oxide 3.0%

[0037] ITX photoinitiator 2.0%

[0038] Sodium polyacrylate 1.0%

[0039] Sodium Carboxymethyl Cellulose 0.1%

[0040] Calcium Stearate Emulsion 0.1%

[0041] Dimethicone 0.1%

[0042] Talc 16.0%

[0043] Solvent amount

[0044] (2) According to Bi(NO 3 ) 3 .5H 2 O, EDTA and NH 4 VO 3 The molar ratio is 1:0.3:1 ratio, weigh Bi(NO 3 ) 3 .5H 2 O dissolved in HNO 3 In the aqueous solution, heat and stir at 85°C for 15 minutes until clear, then add ethylenediaminetetraacetic acid (EDTA); at the same time, weigh the corresponding NH 4 VO 3 Dissolve in deionized water, heat and stir at 45°C for 15 minutes until clarified; mix the above two solutions under constant stirring, adjust the pH to 4.0, and obtain BiVO 4 Precursor solution, spare;

...

Embodiment 2

[0050] 1. Preparation of light-resistant graphene UV ink

[0051] (1) Raw material ratio is as follows (mass fraction):

[0052] Urethane Acrylic 36%

[0053] Photocatalytic modified graphene 5.0%

[0054] Chrome Yellow 4.0%

[0055] 184 Photoinitiator 1.5%

[0056] Sodium polyacrylate 1.0%

[0057] Sodium Carboxymethyl Cellulose 0.1%

[0058] Calcium Stearate Emulsion 0.1%

[0059] Dimethicone 0.1%

[0060] Talc 20.0%

[0061] Solvent amount

[0062] (2) According to Bi(NO 3 ) 3 .5H 2 O, EDTA and NH 4 VO 3 The molar ratio is 1:0.3:1, weigh Bi(NO 3 ) 3 .5H 2 O dissolved in HNO 3 In the aqueous solution, heat and stir at 85°C for 15 minutes until clear, then add ethylenediaminetetraacetic acid (EDTA); at the same time, weigh the corresponding NH 4 VO 3 Dissolve in deionized water, heat and stir at 45°C for 15 minutes until clarified; mix the above two solutions under constant stirring, adjust the pH to 4.0, and obtain BiVO 4 Precursor solution, spare;

[0063...

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Abstract

The invention discloses light-resistant graphene UV ink and a preparation method thereof. The light-resistant graphene UV ink comprises light-resistant graphene UV ink; and the light-resistant graphene UV ink is prepared from polyurethane acrylic resin, photocatalytic modified graphene, pigment, a photoinitiator, a dispersing agent, an auxiliary and filler. The specific preparation process comprises the following steps: weighing a certain amount of Bi(NO3)3.5H2O, dissolving the Bi(NO3)3.5H2O in an HNO3 aqueous solution, adding ethylenediamine tetraacetic acid (EDTA) with a certain concentration, meanwhile, weighing a certain amount of NH4VO3, dissolving the NH4VO3 in deionized water, and conducting heating and stirring at 45 DEG C until the solution is clear, so as to obtain a BiVO4 precursor solution; step 2, preparing photocatalytic graphene UV ink, and conducting storing in a dark place; and step 4, filtering the photocatalytic graphene UV printing ink, adding the filtered photocatalytic graphene UV printing ink into an ink fountain, and carrying out PVC film unwinding, intaglio printing (coating), air box drying, UV curing, protective layer coating, air box drying and winding to obtain a finished product. A high-temperature and high-pressure reaction kettle is adopted for preparation, blending and storage are performed under the dark condition, the preparation process is simple, the yield is high, the product validity period is long, and the method is suitable for industrial production.

Description

technical field [0001] The invention relates to a light-resistant graphene UV ink and a preparation method thereof, belonging to the technical field of PVC film printing. Background technique [0002] With the improvement of production technology, polyvinyl chloride (PVC) decorative panels are widely used in the field of architectural decoration due to their advantages such as non-flammability, high strength, weather resistance and low processing cost. Direct printing of PVC film refers to printing patterns and patterns of various colors directly on the surface of PVC film through printing process to achieve imitation wood, imitation marble and other effects. It has the characteristics of simple process and less material consumption, and can be greatly improved Improve the added value of PVC decorative panels. [0003] Inks used for direct printing of PVC films are becoming more and more popular due to their advantages of cold curing, fast curing, low volatility, environmen...

Claims

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Application Information

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IPC IPC(8): C09D11/101C09D11/03C09D11/102
CPCC09D11/101C09D11/03C09D11/102
Inventor 周瑾夏登明王向锋
Owner 南通吉美装饰材料有限公司
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