Plant extract combined dressing based on ginseng extract and preparation method thereof
A plant extract, ginseng extraction technology, applied in medical science, absorbent pads, bandages and other directions, can solve the problems of poor air permeability, wound healing effect, reduce air permeability of chitosan film, etc., achieve good stability, antibacterial and bacteriostatic. Excellent effect, no side effects, bactericidal effect
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Embodiment 1
[0041] A preparation method of a plant extract combination dressing based on ginseng extract, comprising the following steps:
[0042] (1) Take zinc nitrate hexahydrate and ethanol, mix and stir for 20 minutes, add ethyl orthosilicate, stir evenly, and obtain material C;
[0043] Take cetyltrimethylammonium bromide and deionized water, mix and stir for 5 minutes, add ether, ethanol and ammonia water, continue stirring for 30 minutes, slowly add material C and 3-mercaptopropyltrimethoxysilane dropwise, and stir for 4 hours , the product was collected by centrifugation, washed with ethanol and deionized water in sequence, and dried in vacuum at 60°C; after drying, it was transferred to a mixed solution of ethanol and hydrochloric acid, refluxed at 68°C for 24 hours, washed and dried to obtain mesoporous silica.
[0044] Take mesoporous silica and N,N-dimethylformamide, ultrasonically disperse for 10 minutes to obtain material B; take KH-550, succinic anhydride and N,N-dimethylfo...
Embodiment 2
[0053] A preparation method of a plant extract combination dressing based on ginseng extract, comprising the following steps:
[0054] (1) Take zinc nitrate hexahydrate and ethanol, mix and stir for 25 minutes, add ethyl orthosilicate, stir evenly, and obtain material C;
[0055] Take cetyltrimethylammonium bromide and deionized water, mix and stir for 8 minutes, add ether, ethanol and ammonia water, continue stirring for 35 minutes, slowly add material C and 3-mercaptopropyltrimethoxysilane dropwise, and stir for 5 hours , the product was collected by centrifugation, washed with ethanol and deionized water in sequence, and dried in vacuum at 63°C; after drying, it was transferred to a mixed solution of ethanol and hydrochloric acid, refluxed at 69°C for 22 hours, washed and dried to obtain mesoporous silica.
[0056] Take mesoporous silica and N,N-dimethylformamide, ultrasonically disperse for 13 minutes to obtain material B; take KH-550, succinic anhydride and N,N-dimethylfo...
Embodiment 3
[0065] A preparation method of a plant extract combination dressing based on ginseng extract, comprising the following steps:
[0066] (1) Take zinc nitrate hexahydrate and ethanol, mix and stir for 30 minutes, add ethyl orthosilicate, stir evenly, and obtain material C;
[0067] Take cetyltrimethylammonium bromide and deionized water, mix and stir for 10 minutes, add ether, ethanol and ammonia water, continue stirring for 40 minutes, slowly add material C and 3-mercaptopropyltrimethoxysilane dropwise, and stir for 6 hours , the product was collected by centrifugation, washed with ethanol and deionized water in turn, and dried in vacuum at 65°C; after drying, it was transferred to a mixed solution of ethanol and hydrochloric acid, refluxed at 70°C for 20 hours, washed and dried to obtain mesoporous silica.
[0068] Take mesoporous silica and N,N-dimethylformamide, ultrasonically disperse for 15 minutes to obtain material B; take KH-550, succinic anhydride and N,N-dimethylforma...
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