Energy slow-release cereal-like microspheres, and preparation method and application thereof
A slow-release, grain-based technology, applied in the field of energy slow-release pseudo-grain microspheres and its preparation, to achieve good water absorption and expansibility, and to promote development
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Embodiment 1
[0050] Mix 1g of starch with 5mL of 0.8% sodium alginate solution and 5mL of 1% gellan gum solution, drop the mixed solution into 100mL of 0.2% chitosan solution through the syringe needle through a constant flow pump, and let the mixed solution stand for 1h to make The droplet reacted fully with chitosan to form a gel spherical structure, then filtered out the chitosan solution with gauze, dried the microspheres in an oven at 40°C, and the slow digestible starch content of the obtained microspheres was 49.12%. It shows that the addition of sodium alginate, gellan gum and chitosan can form a polyelectrolyte complex gel film wall covering starch, making it difficult for starch to diffuse into the solution through the gel film. As synthetic or natural macromolecules containing ionizable groups, polyelectrolytes can form a macromolecular polyelectrolyte complex by establishing electrostatic interactions with oppositely charged polyelectrolytes. The formation of polyelectrolyte co...
Embodiment 2
[0052] Mix 1g of starch with 5mL of 0.2% sodium alginate solution and 5mL of 1% gellan gum solution, drop the mixed solution into 100mL of 0.2% chitosan solution through the syringe needle through a constant flow pump, and let the mixed solution stand for 1 hour to make The droplet reacted fully with chitosan to form a gel spherical structure, then filtered out the chitosan solution with gauze, dried the microspheres in an oven at 40°C, and the slow digestible starch content of the obtained microspheres was 34.15%. Sodium alginate has excellent gel properties. Ion exchange occurs in the presence of metal divalent cations, causing guluronic acid to fold and accumulate to form a new hydrophilic space. Metal cations occupy this space and chelate with carboxyl oxygen. , so that the stretched molecular chains are transformed into an ordered ribbon structure, and finally present a three-dimensional network structure of the "egg box" gel. It shows that the polyelectrolyte complex const...
Embodiment 3
[0054] Mix 1g of starch with 5mL of 1% sodium alginate solution and 5mL of 0.6% gellan gum solution, drop the mixed solution into 100mL of 0.2% chitosan solution through the syringe needle through a constant flow pump, and let the mixed solution stand for 1h to make The droplet and chitosan fully reacted to form a gel spherical structure, and then the chitosan solution was filtered out with gauze, and the microspheres were dried in an oven at 40°C. The obtained microspheres had a slow digestible starch content of 47.48%. Gellan gum is an extracellular anionic polysaccharide produced by Pseudomonas chrysophyta. Non-toxic and harmless, it has the viscous properties similar to food gums such as xanthan gum and carrageenan, and can be used as a stabilizer and thickener in food processing industries such as fruit juice and minced meat. Gellan gum also has good gel properties. After heating and dissolving gellan gum, after cooling, the linear molecules will automatically rearrange i...
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