Wetting reversal agent for acidification, preparation method, and construction method thereof in sandstone geothermal reservoir
A wetting inversion and emulsifier technology, which is applied in the field of wetting inversion agent for sandstone geothermal reservoir construction, preparation, and acidification, can solve the problems of hindering water production, achieve low cost, good compatibility, and inhibit retention Effect
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Embodiment 1
[0049] A wetting reversal agent, which is prepared by the following steps:
[0050] S1. Add 2.4 mol of sodium dodecylbenzenesulfonate to 600 mL of water, then add 1.2 mol of sodium carbonate, and stir for 30 min at a speed of 500 to 550 r / min to obtain an emulsifier mixture;
[0051] S2. Pump nitrogen at a rate of 0.2 L / min, add 2 mol of monomer A and 1 mol of monomer B to the emulsifier mixture under nitrogen atmosphere, and use a shear emulsification stirrer to make monomer A and monomer B Mix and stir with the emulsifier mixed solution for 15 minutes at a rotating speed of 300r / min to obtain a prefabricated reaction solution;
[0052] Wherein, the chemical structural formula of monomer A is: R 1 for -CH 3 , R 2 for -CH 3 ; The chemical structural formula of monomer B is: n is 1;
[0053] S3. Transfer the prefabricated reaction solution to the reaction container, and pass nitrogen protection at a rate of 0.2L / min, maintain a stirring speed of 300r / min, and raise the...
Embodiment 2
[0057] A wetting reversal agent, which is prepared by the following steps:
[0058] S1. Add 1.2 mol of sodium dodecylbenzenesulfonate and 1.2 mol of Span-60 to 600 mL of water, then add 1.2 mol of sodium carbonate, and stir for 30 minutes at a speed of 500 to 550 r / min to obtain an emulsifier mixture ;
[0059] S2. Pump nitrogen at a rate of 0.2 L / min, add 2 mol of monomer A and 1 mol of monomer B to the emulsifier mixture under nitrogen atmosphere, and use a shear emulsification stirrer to make monomer A and monomer B Mix and stir with the emulsifier mixed solution for 15 minutes at a rotating speed of 200r / min to obtain a prefabricated reaction solution;
[0060] Wherein, the chemical structural formula of monomer A is: R 1 for-C 3 h 7 , R 2 for R 4 for-C 3 h 7 ; The chemical structural formula of monomer B is: n is 2;
[0061] S3. Transfer the prefabricated reaction solution to the reaction container, and pass nitrogen protection at a rate of 0.2L / min, maint...
Embodiment 3
[0065] A wetting reversal agent, which is prepared by the following steps:
[0066] S1. Add 1.8 mol of sodium dodecylbenzenesulfonate and 1.8 mol of Span-80 to 600 mL of water, then add 2.4 mol of sodium bicarbonate, and stir for 30 minutes at a speed of 500 to 550 r / min to obtain emulsification agent mixture;
[0067] S2. Pump nitrogen at a rate of 0.2 L / min, add 2 mol of monomer A and 2 mol of monomer B to the emulsifier mixture under nitrogen atmosphere, and use a shear emulsification stirrer to make monomer A and monomer B Mix and stir with the emulsifier mixed solution for 15 minutes at a rotating speed of 300r / min to obtain a prefabricated reaction solution;
[0068] Wherein, the chemical structural formula of monomer A is: R 1 for-C 2 h 5 , R 2 for R 4 for-C 2 h 5 ; The chemical structural formula of monomer B is: n is 2;
[0069] S3. Transfer the prefabricated reaction solution to the reaction container, and pass nitrogen protection at a rate of 0.2L / mi...
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