Environment-friendly flame-retardant ternary composite material POSS/GO/ZIF-8 and preparation method thereof
A technology of ZIF-8 and composite materials, which is applied in the field of environmentally friendly flame-retardant ternary composite materials POSS/GO/ZIF-8 and its preparation, to achieve the effect of simple process and high feasibility
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Embodiment 1
[0021] Dissolve 1.5 parts by mass of zinc nitrate in 8 parts by mass of deionized water, stir magnetically for 10 minutes, then add 0.3 parts by mass of POSS / GO binary composite material, stir and sonicate for 30 minutes to obtain solution A; 28.7 parts by mass of 2-methylimidazole are dissolved In 80 parts by mass of deionized water, magnetically stirred for 10 minutes to obtain solution B; pour solution B into solution A and stir for 120 minutes; centrifuge at 10,000 r / min for 10 minutes, wash with deionized water several times, and dry at 65°C to obtain POSS / GO / ZIF-8 ternary composite material.
[0022] Wherein, the preparation method of POSS / GO binary composite material:
[0023] Take 38 parts by mass of POSS and ultrasonically disperse them in 60 mL of tetrahydrofuran, and take 60 parts by mass of GO and ultrasonically disperse them in 60 mL of tetrahydrofuran; mix the two solutions evenly, and put them in a water bath at 65°C for 15 hours in a nitrogen atmosphere, and e...
Embodiment 2
[0025] Dissolve 2.3 parts by mass of zinc nitrate in 8 parts by mass of deionized water, stir magnetically for 10 minutes, then add 0.5 parts by mass of POSS / GO binary composite material, stir and sonicate for 30 minutes to obtain solution A; 43.0 parts by mass of 2-methylimidazole is dissolved In 80 parts by mass of deionized water, magnetically stirred for 10 minutes to obtain solution B; pour solution B into solution A and stir for 120 minutes; centrifuge at 10,000 r / min for 10 minutes, wash with deionized water several times, and dry at 65°C to obtain POSS / GO / ZIF-8 ternary composite material.
[0026] Wherein, the preparation method of the POSS / GO binary composite material is the same as that in Example 1.
Embodiment 3
[0028] Dissolve 3.0 parts by mass of zinc nitrate in 8 parts by mass of deionized water, stir magnetically for 10 minutes, then add 0.6 parts by mass of POSS / GO binary composite material, stir and sonicate for 30 minutes to obtain solution A; 57.4 parts by mass of 2-methylimidazole are dissolved In 80 parts by mass of deionized water, magnetically stirred for 10 minutes to obtain solution B; pour solution B into solution A and stir for 120 minutes; centrifuge at 10,000 r / min for 10 minutes, wash with deionized water several times, and dry at 65°C to obtain POSS / GO / ZIF-8 ternary composite material.
[0029] Wherein, the preparation method of the POSS / GO binary composite material is the same as that in Example 1.
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