A kind of modified polyacrylamide and its preparation method and polymer mud
A polyacrylamide and acrylamide technology, which is applied in the field of pile foundation wall protection materials, can solve the problems of inability to use, reduced viscosity, and general products cannot play a good role, achieving the effect of obvious space effect and increasing electronic effect.
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[0030] The first aspect of the present invention discloses a preparation method of modified polyacrylamide, comprising the following steps:
[0031] dissolving the emulsifier, sodium α-alkenyl sulfonate and acrylamide in deionized water, mixing, stirring and dispersing to obtain the first solution in the state of emulsion;
[0032] dissolving allyl mellitic acid ester in deionized water to obtain a second solution;
[0033] The initiator is dissolved in deionized water to obtain a third solution;
[0034] The hydrophobic monomer and acrylic acid are dissolved in deionized water to obtain a fourth solution;
[0035] After the first solution is deoxygenated, the second solution is added dropwise to it, and the temperature is raised to 60-65°C; the third solution and the fourth solution are added dropwise to it at the same time, and the reaction is continued for 5-6h, After adjusting the pH of the system to 7-8, continue to stir and react, purify, and obtain modified polyacryla...
Embodiment 1
[0052] Preparation of modified polyacrylamide: Add 12.6 parts of mellitic acid and 45 parts of acryl alcohol into the flask and stir thoroughly, then slowly add 0.29 parts of concentrated sulfuric acid dropwise, heat the mixture to 130°C, and react for 3 hours. After the reaction, neutralize the unreacted sulfuric acid with 3.2 parts of calcium hydroxide, and filter out the precipitate. Finally, the filtrate was concentrated to obtain allyl mellitic acid ester.
[0053] Take 1 part of sodium lauryl sulfate, 0.2 part of sodium α-alkenyl sulfonate, 18 parts of acrylamide, add 71.87 parts of deionized water and mix them, then stir and disperse quickly, so that the solution is in the state of emulsion, and then deoxygenate in nitrogen. Under protection, add 0.6 parts of allyl mellitic acid ester to 10 parts of deionized water to form a solution, slowly add it dropwise into the system, and raise the temperature to 60-65°C, and at the same time add 0.53 parts of potassium persulfate...
Embodiment 2
[0056] Preparation of modified polyacrylamide: Add 12.6 parts of mellitic acid and 40 parts of acrylic alcohol into the flask and stir thoroughly, then slowly add 0.29 parts of concentrated sulfuric acid dropwise, heat the mixture to 130°C, and react for 3 hours. After the reaction, neutralize the unreacted sulfuric acid with 3.2 parts of calcium hydroxide, and filter out the precipitate. Finally, the filtrate was concentrated to obtain allyl mellitic acid ester.
[0057] Take 0.8 parts of sodium lauryl sulfate, 0.16 parts of sodium α-alkenyl sulfonate, 18 parts of acrylamide and add 71.65 parts of deionized water to mix and then stir and disperse quickly to make the solution in an emulsion state, and then pass nitrogen to remove oxygen. Under protection, add 0.72 parts of allyl mellitic acid ester to 10 parts of deionized water to form a solution, slowly add it dropwise into the system, and raise the temperature to 60-65°C, and add dropwise at the same time with a mass ratio ...
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