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Low-loss optical fiber preform outer cladding, preparation equipment and preparation method thereof, and optical fiber

A technology of optical fiber preform and outer cladding, applied in glass manufacturing equipment, manufacturing tools, etc., can solve the problems of increased Rayleigh scattering, large Rayleigh scattering, and affecting loss, and achieve good optical uniformity and low stress birefringence , high uniformity effect

Inactive Publication Date: 2020-10-30
FUDAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In this technical solution, because quartz sand is used as raw material, its purity and quality consistency is not good, so the prepared preform outer casing will contain the original impurities of quartz sand, which will affect the loss. On the other hand, this solution needs to prepare the outer cladding first. The tube is combined with the mandrel for wire drawing, and the interface structure between the outer cladding sleeve and the mandrel surface is imperfect, which causes Rayleigh scattering to increase, thereby affecting the loss
[0005] The existing outer cladding technology of optical fiber preform is mainly based on external vapor deposition (OVD), which uses SiCl 4 As raw material, through hydrogen and oxygen combustion, high temperature hydrolysis to generate nano-scale SiO 2 The powder is deposited on the surface of the core rod, and then dehydroxylated and sintered into a transparent optical fiber preform in a chlorine atmosphere. The outer cladding density fluctuates greatly after depositing the powder first and then sintering, so the Rayleigh scattering of the optical fiber preform produced by this outer cladding technology is relatively large, making it difficult to obtain better loss

Method used

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  • Low-loss optical fiber preform outer cladding, preparation equipment and preparation method thereof, and optical fiber
  • Low-loss optical fiber preform outer cladding, preparation equipment and preparation method thereof, and optical fiber
  • Low-loss optical fiber preform outer cladding, preparation equipment and preparation method thereof, and optical fiber

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0061] The equipment for preparing the outer coating of the optical fiber preform in the present invention includes a second deposition chamber 9, a first deposition chamber 6, a plasma generator 4, and a quartz torch 3. See figure 1 .

[0062] The second deposition chamber 9 is provided with a second chamber air inlet 10, and an ambient gas storage tank is externally connected to the second chamber air inlet 10, and a target atmosphere is formed in the second deposition chamber 9 through the input of the ambient gas.

[0063] The first deposition chamber 6 is provided inside the second deposition chamber 9, and a first deposition chamber exhaust port 8 and a first deposition chamber intake port 7 are opened on the first deposition chamber exhaust port 8. In communication with the external environment of the second deposition chamber 9, a quartz handle 5 is penetrated through the air inlet 7 of the first deposition chamber. One end of the quartz handle 5 is detachably connected to t...

Embodiment 2

[0074] Adjust the following parameters on the basis of embodiment 1, and the remaining parameters maintain the state of embodiment 1.

[0075] Plasma is used to pre-treat the surface of the core rod before the outer coating is deposited. The core rod rotation speed is 40 rpm, the left and right movement speed of the core rod is 50 mm / min; the distance between the core rod and the torch is 45 mm; the pretreatment is 2 times, and the plasma generator power is 7 kW .

[0076] After reaching the target diameter, the power of the plasma generator is gradually reduced linearly, and the power is reduced for 0.5 hours from the beginning to the time the plasma generator is turned off.

[0077] Test the outer coating of the optical fiber preform and the drawn optical fiber according to the method of Example 1.

Embodiment 3

[0079] On the basis of Embodiment 2, the plasma generator is closed while the air inlet 10 and the air outlet 8 of the second cavity are closed, and the preform is naturally cooled in the first cavity for 1 hour.

[0080] The remaining parameters remain the same as in Example 2.

[0081] Test the outer coating of the optical fiber preform and the drawn optical fiber according to the method of Example 1.

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Abstract

The invention relates to a low-loss optical fiber preform outer cladding, preparation equipment and a preparation method thereof, and an optical fiber. One of four processes of VAD, OVD, MCVD and PCVDis selected to prepare a core rod; plasma is used as a heat source on the surface of the core rod; silicon tetrachloride is subjected to high-temperature oxidation, a high-density silicon dioxide outer cladding layer is generated and deposited on the surface of the core rod; finally, the set target rod diameter is reached; the outer cladding layer has good optical uniformity, high hardness and low stress birefringence, and the 1310 nm attenuation of a G.652D optical fiber preform prepared by the outer cladding method after drawing can reach 0.315 dB / km, and the 1550 nm attenuation can reach 0.175 dB / km. Compared with the prior art, high-temperature plasma is used for pretreating the surface of the core rod, the problem of interface defects is solved, silicon tetrachloride is used as a rawmaterial, high-temperature plasma is used as a heat source, the optical fiber preform outer cladding layer with high compactness, high uniformity and low defects is generated, and the preparation requirement of the low-loss optical fiber preform is met.

Description

Technical field [0001] The invention relates to the technical field of optical fiber communication, in particular to a low-loss optical fiber preform outer cladding, preparation equipment, preparation method and optical fiber. Background technique [0002] The optical fiber preform is divided into two parts: the core rod and the outer cladding. In the existing optical fiber preform manufacturing methods, the axial vapor deposition method (VAD), the external vapor deposition method (OVD), the improved chemical vapor deposition (MCVD) and plasma Bulk chemical vapor deposition (PCVD) can be used for the preparation of core rods; the production methods of the outer coating are mainly concentrated in the RIT / RIC method (tube method), Soot method (external vapor deposition) and external plasma spraying method. RIT The / RIC method is to insert the core rod into the sleeve to directly draw the optical fiber, or to melt it into a solid preform and then draw the wire; the Soot method and t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03B37/018C03B37/027
CPCC03B37/01823C03B37/027
Inventor 钱宜刚沈海平孙耀杰
Owner FUDAN UNIV
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