A kind of preparation method of snowflake pear extract for tobacco
A snow pear and extract technology, applied in the field of flavors and fragrances, can solve the problems of low content of flavonoids and low extraction rate, and achieve the effects of improving extraction rate, high extraction efficiency and improving throat irritation.
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Embodiment 1
[0026] A preparation method of snowflake pear extract for tobacco, comprising the following steps:
[0027] A. Washing the snow pear, peeling and removing the core, cutting into pieces, adding a pretreatment agent, dehydrating after beating to a moisture content of ≤ 2%, and obtaining a snow pear pretreatment;
[0028] The pretreatment agent is formed by mixing ascorbyl palmitate and sorbitol with a mass ratio of 1:7; the amount of the pretreatment agent is 2% of the mass of pear;
[0029] B, take half of the snowflake pear pretreatment, use the volume fraction of 60% ethanol to leach at 45°C for 1.5 hours, filter after cooling, and concentrate to a relative density of 1.2800 to obtain the first extract; the amount of ethanol is 4 times of the amount of pear pretreatment substance;
[0030] C. Take the snowflake pear pretreatment of the other half quality, extract with ethyl propionate at 45°C for 1.5 hours, filter after cooling, and concentrate to a relative density of 1.280...
Embodiment 2
[0033] A preparation method of snowflake pear extract for tobacco, comprising the following steps:
[0034] A. Washing the snow pear, peeling and removing the core, cutting into pieces, adding a pretreatment agent, dehydrating after beating to a moisture content of ≤ 2%, and obtaining a snow pear pretreatment;
[0035] The pretreatment agent is formed by mixing ascorbyl palmitate and sorbitol with a mass ratio of 2:7; the amount of the pretreatment agent is 5% of the mass of snow pear;
[0036] B, take half of the quality snowflake pear pretreatment, use the volume fraction of 60% ethanol to extract at 60 ℃ for 1 hour, filter after cooling, concentrate to a relative density of 1.2880, and obtain the first extract; the consumption of ethanol is snow pear 4 times of the amount of pear pretreatment substance;
[0037] C. Get the other half of the quality snowflake pear pretreatment, leaching with ethyl propionate for 1 hour at 60°C, filter after cooling, and concentrate to a rel...
Embodiment 3
[0040] A preparation method of snowflake pear extract for tobacco, comprising the following steps:
[0041] A. Washing the snow pear, peeling and removing the core, cutting into pieces, adding a pretreatment agent, dehydrating after beating to a moisture content of ≤ 2%, and obtaining a snow pear pretreatment;
[0042] The pretreatment agent is formed by mixing ascorbyl palmitate and sorbitol with a mass ratio of 1:7; the amount of the pretreatment agent is 3% of the mass of pear;
[0043] B, take half of the snowflake pear pretreatment, use the volume fraction of 60% ethanol to extract at 50 ℃ for 1.2 hours, filter after cooling, and concentrate to a relative density of 1.2720 to obtain the first extract; the consumption of ethanol is snow pear 3.5 times of the pear pretreatment substance quality;
[0044] C. Take the snowflake pear pretreatment of the other half of the quality, extract it with ethyl propionate at 50°C for 1.3 hours, filter after cooling, and concentrate to ...
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