Petroleum drilling auxiliary agent and preparation method thereof
A technology for oil drilling and additives, which is applied in the field of petroleum additives to achieve the effects of improving heat resistance and salt resistance, improving heat resistance, and improving heat resistance
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Embodiment 1
[0029]A kind of petroleum drilling aid, in weight part, comprises following raw material: 90 parts of modified humic acid, 25 parts of 4-hydroxyl-6-acetamido-2-naphthalenesulfonic acid, maleic anhydride acylated chitosan 12.5 parts, 7.5 parts of modified potassium hexatitanate whiskers, 1.5 parts of nonylphenol polyoxyethylene ether, 13 parts of linear polyorganopolysiloxane, 7 parts of microcrystalline wax, 4 parts of aluminum hydroxy, 450 parts of water.
[0030] The modified humic acid is obtained by modifying humic acid with polyacrylic acid and a silane coupling agent, and is specifically prepared by the following steps: dissolving polyacrylic acid in ethanol to obtain solution A; Add silane coupling agent KH550, mix evenly to obtain solution B; add humic acid to solution B, disperse evenly by ultrasonic, then raise the temperature to 75°C, react for 4 hours under stirring conditions, filter after the reaction, and dry to obtain the obtained solution Described modified hu...
Embodiment 2
[0036] A petroleum drilling aid, in parts by weight, comprising the following raw materials: 80 parts of modified humic acid, 30 parts of 4-hydroxy-6-acetylamino-2-naphthalenesulfonic acid, maleic anhydride acylated chitosan 10 parts, 10 parts of modified potassium hexatitanate whiskers, 1 part of nonylphenol polyoxyethylene ether, 14 parts of linear polyorganopolysiloxane, 6 parts of microcrystalline wax, 5 parts of aluminum hydroxy, 400 parts of water.
[0037] The modified humic acid is obtained by modifying humic acid with polyacrylic acid and a silane coupling agent, and is specifically prepared by the following steps: dissolving polyacrylic acid in ethanol to obtain solution A; Add silane coupling agent KH550, mix evenly to obtain solution B; add humic acid to solution B, disperse evenly by ultrasonic, then raise the temperature to 62°C, react for 4.3h under stirring conditions, filter and dry after the reaction is complete, to obtain The modified humic acid; wherein, th...
Embodiment 3
[0043] A petroleum drilling aid, in parts by weight, comprising the following raw materials: 100 parts of modified humic acid, 20 parts of 4-hydroxy-6-acetylamino-2-naphthalenesulfonic acid, maleic anhydride acylated chitosan 15 parts, 5 parts of modified potassium hexatitanate whiskers, 2 parts of nonylphenol polyoxyethylene ether, 10 parts of linear polyorganopolysiloxane, 10 parts of microcrystalline wax, 3 parts of aluminum hydroxy, 500 parts of water.
[0044] The modified humic acid is obtained by modifying humic acid with polyacrylic acid and a silane coupling agent, and is specifically prepared by the following steps: dissolving polyacrylic acid in ethanol to obtain solution A; Add silane coupling agent KH550, mix evenly to obtain solution B; add humic acid to solution B, disperse evenly by ultrasonic, then raise the temperature to 80°C, react for 4.2h under stirring conditions, filter and dry after the reaction is complete, to obtain The modified humic acid; wherein, ...
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Abstract
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