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Micro-water dyeing method suitable for wool

A dyeing method and wool technology, applied in the field of dyeing, can solve the problems of limited varieties and no industrial application, and achieve the effects of improving utilization rate, reducing hydrolysis and low water consumption

Active Publication Date: 2020-07-28
HAINING GREEN UNIVERSE TEXTILE TECH CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the reactive disperse dye supercritical CO 2 Dyeing is only in the research and development stage, and the types of dyes suitable for this dyeing system are limited, and there is no large-scale industrial application at present

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] A dyeing method suitable for wool, the method steps are:

[0030] a, prepare the product to be dyed; prepare 1kg undyed wool top;

[0031] b. Configure a special dyeing system: dissolve 3% (owf) reactive red 195 in 1.5kg of aqueous solution, stir evenly, add 10kg of siloxane to prepare a special dyeing system;

[0032] c. Dyeing: Put the wool products and special dyeing system into the dyeing vat, after 15 minutes of circulation, raise the temperature to 80°C at 2°C / min, and keep it warm for 60 minutes;

[0033] d. Soaping: The soaping is a neutral soaping agent, the dosage is 2g / L, the bath ratio is 1:10, the soaping temperature is 90°C, the soaping time is 20min, and after soaping, wash in hot water at 60°C for 20min;

[0034] e. Dehydration: Put the dyed wool products into the dehydrator for dehydration, and use the recovery device to recycle the poor solvent in the dehydrator;

[0035] f. Drying: Dry the dehydrated wool products through a dryer to obtain dyed prod...

Embodiment 2

[0038] A micro-water dyeing method suitable for wool, the method steps are:

[0039] a, prepare the product to be dyed; prepare 1kg undyed wool top;

[0040] b. Configure a special dyeing system: dissolve 2% (owf) black C-BS in 1.0kg aqueous solution, stir evenly, add 10kg decamethylcyclopentasiloxane (D5) to prepare a special dyeing system;

[0041] c. Dyeing: put wool products and special dyeing system into the dyeing vat, after 15 minutes of circulation, raise the temperature to 95°C at 1°C / min, and keep it warm for 60 minutes;

[0042] Before heating up, add 2% owf wool swelling agent, 1% owf penetrating agent, acetic acid to adjust pH=5, raise the temperature to 70°C and keep it warm for 20min.

[0043] d. Soaping: The soaping is a neutral soaping agent, the dosage is 1g / L, the bath ratio is 1:10, the soaping temperature is 90°C, the soaping time is 30min, and after soaping, wash in hot water at 60°C for 10min;

[0044] e. Dehydration: Put the dyed wool products into th...

Embodiment 3

[0047] A micro-water dyeing method suitable for wool, the method steps are:

[0048] a, prepare the product to be dyed; prepare 1kg undyed wool top;

[0049] b. Configure a special dyeing system: dissolve 2% (owf) black C-BS in 1.0kg aqueous solution, stir evenly, add 10kg of paraffin to prepare a special dyeing system;

[0050] c. Dyeing: Put the wool products and special dyeing system into the dyeing vat, after 15 minutes of circulation, raise the temperature to 95°C at 1°C / min, and keep it warm for 80 minutes;

[0051] Before heating up, add 2% owf wool swelling agent, 1% owf penetrating agent, acetic acid to adjust pH=5, raise the temperature to 70°C and keep it warm for 20min.

[0052] d. Soaping: The soaping is a neutral soaping agent, the dosage is 3g / L, the bath ratio is 1:15, the soaping temperature is 90°C, the soaping time is 15min, and after soaping, wash with hot water at 55°C for 20min;

[0053] e. Dehydration: Put the dyed wool products into the dehydrator for...

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Abstract

The invention relates to a micro-water dyeing method suitable for wool. The micro-water dyeing method comprises the following steps that a, products to be dyed are prepared; b, a dedicated dyeing system is configured, specifically, reactive dyes and metered water only used for dissolving the reactive dyes are uniformly stirred, and poor solvents of the reactive dyes are added to prepare the dedicated dyeing system; c, dyeing is carried out; d, soaping is carried out; e, dehydrating is carried out; and f, drying is carried out, and dyeing products are obtained. Compared with a traditional woolreactive dyeing method, the dyeing method does not require any accelerating salt, with the help of non-aqueous media with low surface tension, the reactive dyes can be rapidly dyed to the surfaces ofwool fibers, the reactive dyes hardly hydrolyze without an alkaline agent, and the fixation rate of the reactive dyes is greatly improved. According to the micro-water dyeing method suitable for the wool, the use ratio of the reactive dyes for wool dyeing is effectively improved, the dyed wool is not required to be specifically processed, and the wet rubbing fastness meets the requirements in themarket.

Description

technical field [0001] The invention relates to a dyeing method, in particular to a micro-water dyeing method suitable for wool, and belongs to the technical field of dyeing. Background technique [0002] In recent years, the application of wool-specific reactive dyes has become more and more common. However, because wool structure is one of the most complex natural fibers, the surface is covered with scales and is hydrophobic. The dye solution is not easy to diffuse into the fiber, which hinders the adsorption and diffusion of dyes. , the dye is difficult to dye to the fiber. Especially for some dyes with low affinity, the dye concentration in the raffinate is relatively high, and the sewage treatment is difficult. Therefore, wool dyeing generally adopts higher temperature and longer dyeing time, resulting in higher energy consumption during dyeing and greater damage to fibers, especially when dyeing outside the isoelectric point of wool, the damage to wool is greater. Ro...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P3/14D06P1/38D06P1/81D06P1/92D06P5/02
CPCD06P3/148D06P1/38D06P5/02D06P1/81D06P1/928D06P1/926
Inventor 王际平裴刘军刘今强
Owner HAINING GREEN UNIVERSE TEXTILE TECH CO LTD
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