Graphene mixed filler, preparation method thereof, graphene mixed filler chromatographic column and application
A technology of mixing filler and graphene, applied in the field of analytical chemistry, can solve the problems of easy agglomeration, target separation and inconvenient elution
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Embodiment 1
[0027] Embodiment 1: the preparation of graphene mixed alumina chromatography column
[0028] 25 parts by weight of the graphene powder with a particle size of 3000-5000 mesh are added with water and stirred evenly to make a graphene suspension;
[0029] Adding 100 parts by weight of the graphene suspension to alumina with a particle size of 200-500 meshes, mixing evenly, and drying at 90° C. for 2-5 hours to obtain a graphene mixed medium filler;
[0030] The lower part of the chromatographic column is filled with alumina with a particle size of 200-500 mesh, the height of the lower part of the chromatographic column accounts for 8% of the height of the chromatographic column, and the upper part of the chromatographic column is filled with graphene mixed media filler, the chromatographic column The ratio of diameter to height is 1:15.
Embodiment 2
[0031] Embodiment 2: the preparation of graphene mixed silica gel chromatography column
[0032] 10 parts by weight of graphene with a particle size of 1000-3000 mesh and a concentration of 50 wt% ethanol aqueous solution are stirred evenly to make a graphene suspension;
[0033] Add 100 parts by weight of the graphene suspension to chromatographic silica gel with a particle size of 200-500 mesh, mix well and then dry at 100°C for 2-5 hours to obtain a graphene mixed media filler; graphene can form a rigid silica gel medium The cage frame immobilizes itself.
[0034]The lower part of the chromatographic column is filled with a particle size of 200-500 mesh chromatographic silica gel, the height of the lower part of the chromatographic column accounts for 5% of the height of the chromatographic column, and the upper part of the chromatographic column is filled with a graphene mixed media filler, the chromatographic column The ratio of diameter to height is 1:25.
Embodiment 3
[0035] Embodiment 3 The preparation of graphene mixed octadecyl bonded silica gel chromatography column:
[0036] 30 parts by weight of graphene powder with a particle size of 3000-5000 mesh is added to 100 parts by weight of octadecyl bonded silica gel with a particle size of 200-500 mesh and mixed uniformly to obtain a graphene mixed medium filler;
[0037] The lower part of the chromatographic column is filled with octadecyl bonded silica gel, the height of the lower part of the chromatographic column accounts for 8% of the height of the chromatographic column, and the upper part of the chromatographic column is filled with graphene mixed medium filler, the diameter of the chromatographic column The height ratio is 1:15.
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