Preparation method and application of mosaic type magnetic imprinting adsorbent
A technology of imprinted adsorption and mosaic, applied in chemical instruments and methods, other chemical processes, alkali metal oxides/hydroxides, etc., can solve the problems of site loss, difficult separation and collection, selectivity to be improved, etc., to achieve improved Effects of selective, easy-to-separate collection
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Embodiment 1
[0045] (1) Fe 3 o 4 -NH 2 preparation of
[0046] 1.0g FeCl 3 ·6H 2 O, 6.5g of 1,6-hexanediamine, 2.0g of anhydrous sodium acetate and 30mL of ethylene glycol were stirred and became transparent at 50°C. The mixture was transferred to an autoclave and heated to 200 °C for 6 hours. After the reaction, wash the black amino-modified Fe with water and ethanol 3 o 4 Nanoparticles (Fe 3 o 4 -NH 2 ) and separated by a magnet, and dried under vacuum at 50°C. The product was redispersed in toluene at a concentration of 10 mg / mL.
[0047] (2) Preparation of J-SNs nanosheets;
[0048] by Hummer ’ s method to prepare GO nanosheets. 50mg GO nanosheets were used as stable particles, 50mL water and 5g solid paraffin were used as continuous phase and dispersed phase respectively, 3.75mL saturated sodium chloride (NaCl) solution was added as electrolyte, and stirred at a high speed of 14000rpm for 5min to generate GO stable Pickering Emulsion (GO-Pickering). It was then collect...
Embodiment 2
[0059] (1) Fe 3 o 4 -NH 2 preparation of
[0060] 1.0g FeCl 3 ·6H 2 O, 6g of 1,6-hexanediamine, 1.5g of anhydrous sodium acetate and 20mL of ethylene glycol were stirred at 50°C and became transparent; the mixture was transferred to an autoclave and heated to 200°C for 6h. After the reaction, wash the black amino-modified Fe with water and ethanol 3 o 4 Nanoparticles (Fe 3 o 4 -NH 2 ) and separated by a magnet, and dried under vacuum at 50°C. The product was redispersed in toluene at a concentration of 10 mg / mL.
[0061] (2) Preparation of J-SNs nanosheets;
[0062] by Hummer ’ GO nanosheets were prepared by s method; 50mg GO nanosheets were used as stable particles, 40mL water and 4g solid paraffin were used as continuous phase and dispersed phase respectively, and 3.5mL saturated sodium chloride (NaCl) solution was added as electrolyte, and stirred at a high speed at 14000rpm After 5 minutes, a GO-stabilized Pickering emulsion (GO-Pickering) was generated. It w...
Embodiment 3
[0068] (1) Fe 3 o 4 -NH 2 preparation of
[0069] 1.0g FeCl 3 ·6H 2 O, 7g of 1,6-hexanediamine, 2.5g of anhydrous sodium acetate and 40mL of ethylene glycol were stirred at 50°C and became transparent. The mixture was transferred to an autoclave and heated to 200 °C for 6 h. After the reaction, wash the black amino-modified Fe with water and ethanol 3 o 4 Nanoparticles (Fe 3 o 4 -NH 2 ) and separated by a magnet, and dried under vacuum at 50°C. The product was redispersed in toluene at a concentration of 10 mg / mL.
[0070] (2) Preparation of J-SNs nanosheets;
[0071] by Hummer ’ s method to prepare GO nanosheets. 50mg GO nanosheets were used as stable particles, 60mL water and 6g solid paraffin were used as continuous phase and dispersed phase respectively, 4mL saturated sodium chloride (NaCl) solution was added as electrolyte, and stirred at a high speed of 14000rpm for 5min to generate GO stable Pickering emulsion (GO-Pickering). It was then collected by cen...
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