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Suspension point contact type supercritical extraction device

An extraction device and supercritical technology, which is applied in the field of suspended point contact supercritical extraction device, can solve the problems of lower extraction efficiency, higher extraction cost, and lower extraction rate, so as to improve extraction efficiency, increase single-pass extraction rate, and improve extraction rate effect

Pending Publication Date: 2020-06-16
NANTONG HUAAN SUPER CRITICAL EXTRACTION
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  • Abstract
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AI Technical Summary

Problems solved by technology

[0004] The extraction rate of existing supercritical extraction devices generally depends on the extraction effect of the extraction tank and the separation effect of the separator. Due to the characteristics of supercritical fluid, it is easy to achieve a high separation rate from the operation of changing temperature and pressure, even Multi-stage separation and rectification are used to improve the separation effect, but most of the extraction kettles still use simple hanging baskets to hold the materials for static extraction. Due to the accumulation and limited space of the materials, it is difficult to carry out the separation process with the supercritical fluid. Sufficient contact leads to a low single-pass extraction rate. It is often necessary to use repeated extraction or continuous countercurrent extraction to increase the extraction rate of the material, which greatly reduces the extraction efficiency and increases the extraction cost.

Method used

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  • Suspension point contact type supercritical extraction device
  • Suspension point contact type supercritical extraction device
  • Suspension point contact type supercritical extraction device

Examples

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Embodiment 1

[0042] see figure 1 , a suspended point contact supercritical extraction device, comprising a carbon dioxide cylinder 1, a purifier 2, a condenser 3, a main pump 4, a mixer 5, a heater 6, an extraction kettle 7 and a separator 9 connected in sequence, the separator 9 is also connected with liquefaction tank 10, and liquefaction tank 10 is connected with compressor 29, and compressor 29 is connected with carbon dioxide cylinder 1, please refer to figure 2 A multi-layer material cylinder 8 is installed in the extraction kettle 7, and a plurality of evenly distributed distribution plates 11 are fixedly installed in the multi-layer material cylinder 8.

[0043] see image 3 , the upper end of the distribution plate 11 is provided with a plurality of evenly distributed hemispherical troughs 13, and the bottom wall of the hemispherical troughs 13 is provided with an ascending channel 12 passing through the distribution plate 11 to provide a flow channel for the supercritical fluid...

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Abstract

The invention discloses a suspension point contact type supercritical extraction device. The invention belongs to the technical field of supercritical extraction. A hanging basket static extraction mode in a traditional extraction kettle can be abandoned; the deformation characteristic of an empty throwing material receiving film is utilized; contained materials are shaken and thrown in the air; apowdery material is promoted to keep a dispersed suspended state; then, supercritical fluid sequentially passes through a limited space to be in full contact with the materials; the extraction rate of effective substances is obviously improved; through the characteristics of the empty throwing material receiving film and the assisting action of an assisting hanging piece, on one hand, the material dispersion effect is improved, meanwhile, the posture can be changed by overturning, the material is in contact with the supercritical fluid, the materials are fully extracted, and extraction dead corners are not prone to occurring; on the other hand, the situation that the extraction effect is affected due to the static adhesion phenomenon of the powdery materials can be avoided; the one-way extraction rate of the materials can be greatly increased, and the extraction efficiency is greatly improved.

Description

technical field [0001] The invention relates to the technical field of supercritical extraction, and more specifically relates to a suspended point contact type supercritical extraction device. Background technique [0002] Supercritical is a supercritical fluid, which is a state of matter that is neither gaseous nor liquid between gas and liquid. This substance can only exist when its temperature and pressure exceed the critical point. The density of supercritical fluid is relatively high. Large, similar to liquid, and its viscosity is closer to gas, so supercritical fluid is a very ideal extraction agent. In the process of pharmaceuticals, supercritical extraction equipment is generally used to extract the effective substances of Chinese herbal medicine. The principle of supercritical carbon dioxide fluid extraction and separation process is to use the relationship between the dissolving ability of supercritical fluid and its density, that is, to use the influence of press...

Claims

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Application Information

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IPC IPC(8): B01D11/02
CPCB01D11/0203B01D11/0257B01D11/0296
Inventor 金雪松黄顺民金宇张森林周伯荣
Owner NANTONG HUAAN SUPER CRITICAL EXTRACTION
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