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Production process for preparing urea solution for vehicles from industrial urea

A technology for vehicle urea and production process, which is applied in the preparation of urea derivatives, the preparation and dissolution of organic compounds, etc., can solve the problem of reverse osmosis membrane flux and anti-pollution performance limiting production capacity, complex filtration and purification processes, and product quality. It is difficult to meet the needs and other problems, and achieve the effect of realizing large-scale production, meeting the needs of small-batch orders, and low one-time investment cost

Inactive Publication Date: 2020-05-08
安徽德利来环保科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The filtration and purification process of the above-mentioned (2) route is complicated, the equipment investment cost is high, and the reverse osmosis membrane flux and anti-pollution performance of the filtration process limit its production capacity
The (3) route is only suitable for large-scale chemical enterprises producing urea, and the impurities such as ammonia, formaldehyde, and diuresis in the product are relatively high, and the product quality is difficult to meet the requirements.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] A kind of production technology of preparing vehicle urea solution by industrial urea, comprises the following steps:

[0026] S1: Remove impurities for industrial urea. After the removal of impurities, crush the urea raw material in a low-temperature environment, and then mix the raw industrial urea powder with ultrapure water at a temperature of 20°C to completely dissolve industrial urea in ultrapure water. , to obtain industrial urea solution;

[0027] S2, continuously add urea powder to the urea solution in step S1 until the solution reaches saturation, then mix the saturated industrial urea solution with the crystallizer circulating fluid and enter the external crystallization cooler tube together for cooling;

[0028] S3: When the temperature of the saturated industrial urea solution and the crystallizer circulating fluid drops to 5°C, send the cooled industrial urea solution and the crystallizer circulating fluid mixed solution to the crystallizer;

[0029] S4....

Embodiment 2

[0032] A kind of production technology of preparing vehicle urea solution by industrial urea, comprises the following steps:

[0033] S1: Remove impurities for industrial urea. After the removal of impurities, crush the urea raw material in a low-temperature environment, and then mix the raw industrial urea powder with ultra-pure water at a temperature of 25°C to completely dissolve industrial urea in ultra-pure water , to obtain industrial urea solution;

[0034] S2, continuously add urea powder to the urea solution in step S1 until the solution reaches saturation, then mix the saturated industrial urea solution with the crystallizer circulating fluid and enter the external crystallization cooler tube together for cooling;

[0035] S3: When the temperature of the saturated industrial urea solution and the crystallizer circulating fluid drops to 6°C, send the cooled industrial urea solution and the crystallizer circulating fluid mixed solution to the crystallizer;

[0036] S4...

Embodiment 3

[0039] A kind of production technology of preparing vehicle urea solution by industrial urea, comprises the following steps:

[0040] S1: Remove impurities for industrial urea. After the removal of impurities, crush the urea raw material in a low-temperature environment, and then mix the raw industrial urea powder with ultrapure water at a temperature of 30°C to completely dissolve industrial urea in ultrapure water. , to obtain industrial urea solution;

[0041] S2, continuously add urea powder to the urea solution in step S1 until the solution reaches saturation, then mix the saturated industrial urea solution with the crystallizer circulating fluid and enter the external crystallization cooler tube together for cooling;

[0042] S3: When the temperature of the saturated industrial urea solution and the crystallizer circulating fluid drops to 7°C, send the cooled industrial urea solution and the crystallizer circulating fluid mixed solution to the crystallizer;

[0043] S4....

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PUM

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Abstract

The invention discloses a production process for preparing a urea solution for vehicles from industrial urea. The production process comprises the following steps: S1, removing impurities from industrial urea, crushing the urea raw material in a low-temperature environment after the impurities are removed, and then mixing the raw material, namely industrial urea powder with ultrapure water at a temperature of 20-40 DEG , so as to allow the industrial urea powder to be completely dissolved in the ultrapure water to obtain an industrial urea solution; and S2, continuously adding the industrial urea powder into the urea solution obtained in the step S1 until the solution is saturated, then mixing the saturated industrial urea solution and crystallizer circulating liquid, and allowing an obtained mixture to enter an external crystallization cooler pipe for cooling. According to the production process for preparing the urea solution for vehicles from the industrial urea, the cheap industrial urea is used as the raw material, process flow is short, equipment is simple, operation is convenient, and the production process is suitable for mass production.

Description

technical field [0001] The invention relates to the technical field of vehicle urea production technology, in particular to a production process for preparing vehicle urea solution from industrial urea. Background technique [0002] Although the domestic automotive urea solution market has just started, the market demand potential is quite huge, and the sales volume of the domestic automotive urea solution market is growing rapidly. [0003] At present, the domestic production of urea for vehicles is dominated by small and medium-sized private enterprises, and the main production processes are divided into the following three routes: (1) Firstly, urea particles for vehicles are produced by re-purification of industrial urea, and then mixed with ultrapure water in proportion to prepare Urea solution for vehicles; (2) Industrial or agricultural urea is first mixed with ultrapure water, and then the urea solution for vehicles is prepared through the processes of primary filtrat...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01F13/10B01F1/00B01D9/00B01F15/06B01D36/00C07C273/16
CPCB01D9/0004B01D36/003C07C273/16B01F21/02B01F33/83B01F33/83612B01F2035/98B01F35/92B01F2101/48
Inventor 杨海涛杨海波
Owner 安徽德利来环保科技有限公司
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