Detection method of traditional Chinese medicine composition with sleep improving function

A detection method and composition technology, applied in the directions of measuring devices, instruments, scientific instruments, etc., can solve the problems of unfavorable composition internal quality control, no product detection method, inconvenient operation, etc., to reduce detection costs, Time-reducing, specific effects

Active Publication Date: 2020-03-03
PERFECT CHINA +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] For this reason, Chinese patent literature CN102188610A discloses a kind of traditional Chinese medicine composition with sleep-improving function, including extracts such as ganoderma lucidum, longan meat, jujube seed, cypress kernel, Shouwuteng, Polygonatum, and jujube, but it only introduces the The raw material composition and preparation method of the above-mentioned traditional Chinese medicine composition and the corresponding product testing method are not given, which is not conducive to the internal quality control of the composition in the process of production, circulation and use
In the prior art, there are many detection and analysis methods for Ganoderma lucidum and Shouwu Teng. For example, the Chinese journal document "Research on Quality Control Methods for Minerankang Granules" discloses TLC identification methods for Shouwu Teng and Ganoderma lucidum. Considering two The composition and properties of the medicinal materials are quite different, and it is difficult to identify them under the same conditions at the same time. Therefore, the pretreatment methods for Shouwu Teng and Ganoderma lucidum are different in this method, and the developer systems finally selected are also quite different. The developer selected for the former is For the benzene-ethanol system, the developer used in the latter is petroleum ether (60-90°C)-ethyl formate-formic acid system, which is very inconvenient to operate, especially when a large batch of detection is required, the workload is very large and the work efficiency is very high. Low

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  • Detection method of traditional Chinese medicine composition with sleep improving function
  • Detection method of traditional Chinese medicine composition with sleep improving function
  • Detection method of traditional Chinese medicine composition with sleep improving function

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Embodiment 1

[0068] This embodiment 1 provides a kind of quality control method of the traditional Chinese medicine composition with the function of improving sleep, comprising the following steps:

[0069] 1. Identify ganoderma lucidum and Shouwu vine in the Chinese medicine composition with thin-layer chromatography

[0070] Take the traditional Chinese medicine composition for improving sleep function, 5 g of the negative reference substance without the extract of Radix Polygoni Multiflori, 5 g of the negative reference substance without Ganoderma lucidum, 1 g of Ganoderma lucidum extract, and 1 g of Radix Polygoni Multiflori extract, add 30 mL of ethanol, and sonicate for 30 Minutes, filter, evaporate the filtrate to dryness in a water bath, add 1 mL of ethanol to dissolve it, and use it as the test solution, negative control solution and extract solution respectively. In addition, 2 g of Ganoderma lucidum and about 0.25 g of Shouwu Teng reference medicinal materials were taken to make...

Embodiment 2

[0088] This embodiment 2 provides a kind of quality control method of the traditional Chinese medicine composition with the function of improving sleep, comprising the following steps:

[0089] 1. Identify ganoderma lucidum and Shouwu vine in the Chinese medicine composition with thin-layer chromatography

[0090] Take the traditional Chinese medicine composition for improving sleep function, 5 g of the negative control substance without the extract of Shouwu Teng, 5 g of the negative control without Ganoderma lucidum, 1 g of Ganoderma lucidum extract, and 1 g of Shouwu Teng extract, add 20 mL of methanol, and ultrasonicate for 40 Minutes, filter, evaporate the filtrate to dryness in a water bath, add 1.5 mL of propanol to dissolve it, and use it as the test solution, negative control solution and extract solution respectively. In addition, 2 g of Ganoderma lucidum and about 0.25 g of Shouwu Teng reference medicinal materials were taken to make a reference medicinal solution i...

Embodiment 3

[0108] This embodiment 3 provides a kind of quality control method of the traditional Chinese medicine composition with the function of improving sleep, comprising the following steps:

[0109] 1. Identify ganoderma lucidum and Shouwu vine in the Chinese medicine composition with thin-layer chromatography

[0110] Take the traditional Chinese medicine composition for improving sleep function, 5g of the negative control substance without the extract of Radix Polygoni Multiflori, 5g of the negative control substance without Ganoderma lucidum, 1g of Ganoderma lucidum extract, 1g of Radix Radix Polygonum extract, add 40mL of propanol, and perform ultrasonic treatment After 20 minutes, filter, evaporate the filtrate to dryness in a water bath, add 0.5 mL of methanol to dissolve it, and use it as the test solution, negative control solution and extract solution respectively. In addition, 2 g of Ganoderma lucidum and about 0.25 g of Shouwu Teng reference medicinal materials were take...

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Abstract

The invention belongs to the technical field of traditional Chinese medicine detection. The invention discloses a detection method of a traditional Chinese medicine composition with a sleep improvingfunction. According to the method, lucid ganoderma, vines of multiflower knotweed and spina date seeds are identified through thin-layer chromatography, and the content of spinosyn is measured throughhigh performance liquid chromatography. The same pretreatment method is adopted for the lucid ganoderma and the vines of multiflower knotweed. A specific developing solvent system is selected, so that various components in the lucid ganoderma and the vines of multiflower knotweed can be well separated, and the simultaneous identification of the lucid ganoderma and the vines of multiflower knotweed is realized. In each test sample chromatogram, spots with the same color are displayed at positions corresponding to positive reference substance chromatograms, and interference spots do not exist in negative reference substance chromatograms; and therefore, the method disclosed by the invention has relatively strong specificity. With the method adopted, an operation process is simplified; timerequired for identification is shortened; working efficiency is improved; detection cost is reduced; a new thought is provided for the identification of all the components in the traditional Chinese medicine composition by the thin-layer chromatography; and improvement of traditional Chinese medicine quality control standards is facilitated.

Description

technical field [0001] The invention belongs to the technical field of traditional Chinese medicine detection, and in particular relates to a detection method of a traditional Chinese medicine composition capable of improving sleep. Background technique [0002] Sufficient sleep, balanced diet and proper exercise are the three health standards recognized by the international community. One-third of a person's life is spent in sleep. As a necessary process of life, sleep is an indispensable part of health. Sustained sleep disorders can lead to adverse consequences such as physical and mental damage, social and economic losses, including cardiovascular disease, mental disease, low immunity, and even increased mortality, which has become a serious public health problem. [0003] For this reason, Chinese patent literature CN102188610A discloses a kind of traditional Chinese medicine composition with sleep-improving function, including extracts such as ganoderma lucidum, longan ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/90G01N30/02G01N30/06
CPCG01N30/90G01N30/02G01N30/06
Inventor 郁晓艺罗文光欧阳道福梁淑明卜闪闪陈晶温馨颜建章孙静胡瑞连
Owner PERFECT CHINA
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