A kind of preparation method of horizontal well plugging agent
A horizontal well and plugging agent technology, applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of short validity period, poor temperature and salt resistance, etc.
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[0050] A preparation method of horizontal well plugging agent, comprising the following steps:
[0051] A. Take 200g of montmorillonite, place it in 800mL of dilute hydrochloric acid with a mass fraction of 7.5%, stir and make slurry for 12h, after suction filtration and distillation of hydrochloric acid, wash repeatedly with distilled water until the pH is 7.0, put the treated montmorillonite in Dry at 100°C for two days and reserve;
[0052] B. Take 20g of dried montmorillonite in step A, uniformly disperse it in 400mL of deionized water at a stirring speed of 300 rpm, age for 24h, heat up to 65°C, add 6.56g of hexadecyltrimethyl bromide Ammonium chloride, stirred at a high speed of 300rpm for 1.5h; cooled to 25°C, filtered under reduced pressure, washed with pure water, until silver nitrate was added to the filtrate without precipitation, dried in vacuum at 80°C for 12h, ground, crushed and sieved , the sieve mesh number is 325 orders, makes modified montmorillonite (O-MMT...
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