Method for preparing active extract hair-growing product by taking freeze-dried poecilobdella manillensis freeze-dried powder as raw material
A technology of freeze-dried powder and Hirudo phenatinae, applied in medical raw materials derived from leeches/worms, freeze-dried transportation, pharmaceutical formulas, etc., can solve the problems of hair growth products without active extracts, achieve good efficacy, The effect of increasing hair hardness
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Embodiment 1
[0023] Embodiment 1: a kind of method that is the active extract hair growth product of phenanthrene lyophilized powder as raw material, is characterized in that, comprises the following several steps:
[0024] S1. Take 180-220g of fresh live Hirudo phenatinae whole body, weigh it, and record its weight; wash and homogenize the whole body of Hirudo phenanthae;
[0025] S2. Under the condition of vacuum degree of 2-5pa, freeze-dry the slurry; first pre-freeze the slurry at -45°C--55°C for 3.5-4.5 hours, and then within 46-50 hours Gradually raise the temperature from -50°C to 20°C, and keep it at 18°C-22°C for 3-5 hours, and finally obtain the dried material;
[0026] S3, pulverize the dried material, and sieve it through a 40-60 mesh sieve to obtain 28g-36g of freeze-dried powder;
[0027] S4. First add 900-1100 ml of 0.9% NaCl aqueous solution to the freeze-dried powder, stir and extract at room temperature for 1 hour, filter, and collect the filtrate and residue; add 500-70...
Embodiment 2
[0030] Embodiment 2: a kind of method for the active extract hair growth product of phenanthrene lyophilized powder as raw material, is characterized in that, comprises the following several steps:
[0031] S1. Take 90-100g of fresh live Hirudo phenatinae whole body, weigh it, and record its weight; wash and homogenize the whole body of Hirudo phenanthae;
[0032] S2. Under the condition of vacuum degree of 2-3pa, freeze-dry the slurry; first pre-freeze the slurry at -45°C--50°C for 3.5-4.0 hours, and then within 46-48 hours Gradually increase the temperature from -50°C to 20°C, and keep it at 18°C-20°C for 3-4 hours, and finally obtain the dried material;
[0033] S3, pulverize the dried material, and sieve it through a 40-mesh sieve to obtain 14g-18g of freeze-dried powder;
[0034] S4. First add 450-550 ml of 0.9% NaCl aqueous solution to the freeze-dried powder, stir and extract at room temperature for 1 hour, filter, and collect the filtrate and residue; add 250-350 ml o...
Embodiment 3
[0037] Embodiment 3: a kind of method for the active extract hair growth product of phenanthrene lyophilized powder as raw material, it is characterized in that, comprises the following several steps:
[0038] S1. Take 270-330g of fresh live Hirudo phenatinae whole body, weigh it, and record its weight; wash and homogenize the whole body of Hirudo phenanthae;
[0039] S2. Under the condition of vacuum degree of 4-5pa, freeze-dry the slurry; first pre-freeze the slurry at -50°C--55°C for 4.0-4.5 hours, and then within 48-50 hours Gradually increase the temperature from -50°C to 20°C, and keep it at 20°C-22°C for 4-5 hours, and finally obtain the dried material;
[0040] S3, pulverize the dried material, and sieve it through a 60-mesh sieve to obtain 42g-54g of freeze-dried powder;
[0041] S4. First add 1350-1650 ml of 0.9% NaCl aqueous solution to the lyophilized powder, stir and extract at room temperature for 1 hour, filter, and collect the filtrate and residue; add 750-105...
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