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Compound with triarylamine structure as core and preparation method thereof

A compound, triarylamine technology, applied in the field of organic electroluminescent materials, can solve problems such as disparity, and achieve the effects of improving thermal stability, reducing planarity, and optimizing device structure

Active Publication Date: 2019-12-17
JIANGSU SUNERA TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

In addition, for the collocation of OLED devices with different structures, the photoelectric functional materials used have strong selectivity, and the performance of the same material in devices with different structures may be completely different.

Method used

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  • Compound with triarylamine structure as core and preparation method thereof
  • Compound with triarylamine structure as core and preparation method thereof
  • Compound with triarylamine structure as core and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0062] Embodiment 1: the synthesis of compound 1

[0063]

[0064] (1) In a 250ml three-neck flask, under the protection of nitrogen, add 0.01mol reactant A-1, 0.01mol reactant B-1, 150ml toluene and stir to mix, then add 5×10 -5 mol Pd 2 (dba) 3 , 5×10 -5 mol P(t-Bu) 3 , 0.03mol sodium tert-butoxide, heated to 105°C, refluxed for 24 hours, sampling plate, showed no bromide remaining, the reaction was complete; naturally cooled to room temperature, filtered, the filtrate was rotary evaporated to no fraction, passed through a neutral silica gel column , the intermediate product M-1 was obtained, the HPLC purity was 99.66%, and the yield was 86.8%. HRMS(EI): The molecular weight of the material is 410.1539, and the measured molecular weight is 410.1529;

[0065] (2) In a 250ml three-neck flask, under the protection of nitrogen, add 0.01mol of the intermediate product M-1 obtained in step (1) and 0.01mol of reactant C, and stir and mix with 150ml of toluene, then add 5×10...

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Abstract

The invention discloses a compound taking a triarylamine structure as a core as well as a preparation method and application of the compound. The structure of the compound is shown as a general formula (1). The compound provided by the invention has relatively high glass transition temperature and molecular thermal stability, proper HOMO and LUMO energy levels and relatively high mobility, and caneffectively improve the photoelectric property of an OLED device and prolong the service life of the OLED device by optimizing the structure of the device.

Description

technical field [0001] The invention relates to the technical field of organic electroluminescent materials, in particular to a compound containing triarylamine in its structure and a preparation method thereof. Background technique [0002] Organic electroluminescent (OLED: Organic Light Emission Diodes) device technology can be used to manufacture new display products and also can be used to make new lighting products, which is expected to replace the existing liquid crystal display and fluorescent lighting, and has a wide application prospect. [0003] The OLED light-emitting device is like a sandwich structure, including electrode material film layers, and organic functional materials sandwiched between different electrode film layers. Various functional materials are superimposed on each other according to the application to form an OLED light-emitting device. As a current device, when a voltage is applied to the electrodes at both ends of the OLED light-emitting device...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07D307/91C07D405/14C07D405/10C07D471/04C07D403/12H01L51/54H01L51/50H10K99/00
CPCC07D405/10C07D209/86C09K11/06C09K2211/1014C09K2211/1011C09K2211/1029C09K2211/1088H10K85/631H10K85/6574H10K85/6572H10K50/15H10K50/181C07D307/91C07D403/12C07D405/14C07D471/04C07D519/00C07D491/048H10K85/615H10K85/654H10K85/626H10K50/18H10K50/171H10K2101/30
Inventor 李崇张小庆张兆超赵四杰
Owner JIANGSU SUNERA TECH CO LTD
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