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Clausena lansium(Lour.)Skeels extract-containing tobacco flavor and preparation method and application thereof

A technology for tobacco essence and extract, which is applied in the field of preparation of tobacco essence and extract containing yellow bark extract, to achieve the effects of preventing and treating influenza, harmonious and natural aroma, and overall quality improvement

Pending Publication Date: 2019-12-13
CHONGQING CHINA TOBACCO IND CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the application direction of wampum bark extract is mainly in the field of medicine or cosmetic technology, but there are almost no reports on the field of tobacco flavor

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Preparation of yellow peel fruit extract. Crude extraction: Take 500g of yellow peel fruit, add 4L 40Vol% alcohol, crush with a juicer with a power of 1000W for 1 min, heat and reflux for 2 hours at 80℃, and then at 55℃, 100hPa Under conditions, concentrate under reduced pressure to 30% of the original volume to obtain a crude extract of yellow bark fruit extract for use;

[0030] Refining: Take 100g of the prepared crude extract of yellow bark fruit extract, add 6g of proline, and react for 4h under the conditions of pH 7.5 and reaction temperature of 85°C to obtain the yellow bark fruit extract.

[0031] Preparation of yellow bark leaf extract

[0032] Take 500g of yellow bark leaves, dry in an oven at 50℃ for 2h, smash, pass through a 100-mesh sieve, then add 3L of 50Vol% alcohol, heat reflux at 80℃ for 1.5h, then at 55℃, 100hPa conditions, reduce pressure Concentrate to 30% of the original volume to obtain yellow bark leaf extract.

[0033] Preparation of tobacco flavor

[...

Embodiment 2

[0036] Preparation of yellow peel fruit extract Crude extraction: Take 500g of yellow peel fruit, add 5L of 50Vol% alcohol, crush with a juicer with a power of 1000W for 1min, heat and reflux at 80℃ for 2h, then at 55℃, 100hPa Concentrate under reduced pressure to 50% of the original volume under reduced pressure to obtain a crude extract of yellow bark fruit extract for use;

[0037] Refining: Take 100 g of the prepared crude extract of yellow bark fruit extract, add 5 g of glycine, and react for 3 hours under the conditions of pH 8.0 and reaction temperature of 90° C. to obtain the yellow bark fruit extract.

[0038] Preparation of yellow bark leaf extract

[0039] Take 500g of yellow bark leaves, dry them in a 50℃ oven for 2h, smash them, pass a 100-mesh sieve, add 4L 60Vol% alcohol, heat and reflux for 2h at 80℃, then concentrate under reduced pressure at 55℃, 100hPa 35% of the original volume, the yellow bark leaf extract is obtained.

[0040] Preparation of tobacco flavor

[004...

Embodiment 3

[0043] Preparation of yellow peel fruit extract: Crude extraction: Take 500g of yellow peel fruit, add 5L 60Vol% alcohol, crush with a juicer with a power of 1000W for 1min, heat and reflux for 1.5h at 80℃, then at 55℃, Under 100hPa conditions, concentrate under reduced pressure to 40% of the original volume to obtain a crude extract of yellow bark fruit extract for use;

[0044] Refining: Take 100 g of the prepared crude extract of yellow bark fruit extract, add 6 g of leucine, and react for 2 hours under the conditions of pH 8.5 and reaction temperature of 90° C. to obtain the yellow bark fruit extract.

[0045] Preparation of yellow bark leaf extract

[0046] Take 500g of yellow bark leaves, dry them in an oven at 50℃ for 2h, smash them, pass a 100-mesh sieve, add 5L 55Vol% alcohol, heat and reflux for 2h at 80℃, and then concentrate under reduced pressure at 55℃ and 100hPa To 40% of the original volume, a yellow bark leaf extract is obtained.

[0047] Preparation of tobacco flavo...

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PUM

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Abstract

The invention discloses Clausena lansium(Lour.)Skeels extract-containing tobacco flavor and a preparation method and application thereof, and relates to the technical field of tobacco flavor. The Clausena lansium(Lour.)Skeels extract-containing tobacco flavor includes the following components: in parts by weight, 20-50 parts of alcohol of 95% by volume, 5-20 parts of Clausena lansium(Lour.)Skeelsfruit extract, 7-25 parts of Clausena lansium(Lour.)Skeels leaf extract, 0.2-0.8 part of ethyl maltol, 3-8 parts of tree moss concentrate, 0.5-3 parts of tobacco extract, 0.1-0.3 part of methylionone,10-30 parts of honey and the balance propylene glycol, wherein the total weight is 100 parts. The Clausena lansium(Lour.)Skeels extract-containing tobacco flavor can give cigarettes obvious characteristic aroma, the aroma is harmonious and natural, and the texture and sharpness of the aroma are improved; green, ripe and sweet aroma, freshness and elegance are added, so that the overall quality ofcigarette smoking is improved.

Description

Technical field [0001] The invention relates to the technical field of tobacco flavors, in particular to a tobacco flavor containing a yellow peel extract, a preparation method and an application. Background technique [0002] Earlier, people used the extracts of flowers, plants or tea as tobacco additives, and conducted extensive research on improving the quality of cigarettes, increasing the flavor and taste of cigarettes, etc. Some researchers condense the extract of Luo Han Guo under reduced pressure to make additives for cigarettes, and add them to the binder of the polypropylene filter in a certain proportion to make the polypropylene filter, which can enhance the fragrance, improve the comfort of cigarettes and reduce the harm of smoking. Zhang Junsong et al. prepared a new type of hawthorn spice that not only maintains the rich hawthorn characteristic aroma, but also increases the brewing and fruity aroma, with a typical style, and can effectively remove impurities, impro...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24B3/12A24B15/30
CPCC11B9/00C11B9/0003C11B9/0015A24B3/12A24B15/302
Inventor 朱丛戎邱光明刘如灿李朝荣王毅周远祥周胜杨文敏赵玉轩陶文生马明陈小敏栾荣宇王晶
Owner CHONGQING CHINA TOBACCO IND CO LTD
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