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A kind of waste purple miscellaneous copper refining agent and its preparation method and application

The technology of refining agent and purple miscellaneous copper is applied in the field of waste miscellaneous copper refining agent and its preparation. The effect of sufficient deoxygenation reaction and shortened reaction period

Active Publication Date: 2021-09-07
四川博鑫铜业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The technical problem to be solved by the present invention is that the traditional refining agent has poor impurity removal effect, and the traditional refining process has disadvantages such as long refining time and poor refining effect.

Method used

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  • A kind of waste purple miscellaneous copper refining agent and its preparation method and application

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0042] Place the electrolytic copper with a purity of 99.99%-99.999% in a vacuum melting furnace. After the electrolytic copper is melted, the temperature of the melt is controlled at 1150-1200°C, and the vacuum is evacuated to 10 -2 Pa~10 -3Pa. Stop vacuuming, and pass into a high-purity inert gas with a purity of 99.999%, control the pressure in the furnace to be 1.0 atmospheric pressure, and use the following parts by weight of 25-30% parts of Cu-Mg alloy of Mg, 25-30% of parts of B Cu-B alloy, 50-65% Ce Cu-Ce alloy, 35-50% Y Cu-Y alloy, 35-50% Pr Cu-Pr alloy and 35-50% La Cu- La alloy and other intermediate alloys are put into the copper melt, kept at a temperature range of 1150-1200°C for 20 minutes, poured into a water-cooled iron mold to obtain a refining agent for copper, and the prepared refining agent is 3.8-5.3 parts by weight. B, 4.0-4.8 parts of Mg, 8.5-11 parts of Ce, 6.5-7.5 parts of Pr, 5 parts of Y, 5 parts of La. Take 100kg of waste red miscellaneous coppe...

Embodiment 2

[0044] Place the electrolytic copper with a purity of 99.99%-99.999% in a vacuum melting furnace. After the electrolytic copper is melted, the temperature of the melt is controlled at 1150-1200°C, and the vacuum is evacuated to 10 -2 Pa~10 -3 Pa. Stop vacuuming, and pass into a high-purity inert gas with a purity of 99.999%, control the pressure in the furnace to be 1.0 atmospheric pressure, and use the following parts by weight of 25-30% parts of Cu-Mg alloy of Mg, 25-30% of parts of B Cu-B alloy, 50-65% Ce Cu-Ce alloy, 35-50% Y Cu-Y alloy, 35-50% Pr Cu-Pr alloy and 35-50% La Cu- La alloy and other intermediate alloys are put into the copper melt, kept at a temperature range of 1150-1200°C for 20 minutes, poured into a water-cooled iron mold to obtain a refining agent for copper, and the prepared refining agent is 3.8-5.3 parts by weight. B, 4.0-4.8 parts of Mg, 8.5-11 parts of Ce, 6.5-7.5 parts of Pr, 3 parts of Y, 3 parts of La. Take 100kg of waste red miscellaneous copp...

Embodiment 3

[0046] Place the electrolytic copper with a purity of 99.99%-99.999% in a vacuum melting furnace. After the electrolytic copper is melted, the temperature of the melt is controlled at 1150-1200°C, and the vacuum is evacuated to 10 -2 Pa~10 -3 Pa. Stop vacuuming, and pass into a high-purity inert gas with a purity of 99.999%, control the pressure in the furnace to be 1.0 atmospheric pressure, and use the following parts by weight of 25-30% parts of Cu-Mg alloy of Mg, 25-30% of parts of B Cu-B alloy, 50-65% Ce Cu-Ce alloy, 35-50% Y Cu-Y alloy, 35-50% Pr Cu-Pr alloy and 35-50% La Cu- La alloy and other intermediate alloys are put into the copper melt, kept at a temperature range of 1150-1200°C for 20 minutes, poured into a water-cooled iron mold to obtain a refining agent for copper, and the prepared refining agent is 3.8-5.3 parts by weight. B, 4.0-4.8 parts of Mg, 8.5-11 parts of Ce, 6.5-7.5 parts of Pr, 3.2 parts of Y, 3.2 parts of La. Take 100kg of waste red miscellaneous ...

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Abstract

The invention discloses a waste red miscellaneous copper refining agent and application thereof, and relates to the field of metal smelting. A waste copper refining agent, comprising chemical components in parts by weight: 3.8-5.3 parts of B, 4.0-4.8 parts of Mg, 8.5-11 parts of Ce, 6.5-7.5 parts of Pr, characterized in that it also includes chemical The parts by weight of the components are: 2-5 parts of Y and 2-5 parts of La. The application of a refining agent for waste red miscellaneous copper includes: adding waste red miscellaneous copper into a reverberatory furnace for smelting, and the reverberatory furnace adopts a combustion control system for heat supply, and the temperature of the control liquid is kept at 1155-1165°C; The copper liquid is removed, deoxidized, and purified; the purified copper liquid is placed in a standing furnace for standing still and then deoxidized. The advantages and beneficial effects of the present invention: Y and La elements are added to the refining agent formula for synergistic modification, and the prepared compound refining agent can improve the impurity removal effect of red copper; the thermal cycle design greatly reduces the time required for the process and shortens the reaction cycle.

Description

technical field [0001] The invention relates to the field of metal smelting, in particular to a waste copper refining agent and its preparation method and application. Background technique [0002] With the rapid development of the national economy, my country's demand for copper and copper alloy products is increasing. At present, my country has become the world's largest copper consumer, with copper consumption accounting for 40% of the world's total. However, my country's copper resources are very scarce, and the reserves of copper resources only account for 5% of the world's total. We must rely on imported copper concentrates, electrolytic copper, copper materials and scrap copper to obtain metallic copper, and the cost is relatively high. In fact, copper is a metal material with good regeneration performance. Improving and improving the recycling technology of scrap copper is an effective way to alleviate the shortage of copper resources. [0003] Red miscellaneous co...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C1/06C22C1/03C22C9/00C22B9/10C22B15/04F27B3/20F27B3/28
CPCC22B9/10C22B15/0036C22C1/03C22C1/06C22C9/00F27B3/205F27B3/28Y02P10/143Y02P10/20
Inventor 赵小平黄伟萍饶红张代强
Owner 四川博鑫铜业有限公司
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