Impregnating agent and preparation method and application thereof
A technology of sizing agent and coupling agent, applied in the field of sizing agent for direct yarn for high-quality surface pultrusion profiles
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[0070] The preparation method of this sizing agent comprises the following steps:
[0071] Dilution of 1S film former, surfactant A and surfactant B:
[0072] Dilute the film-forming agent with 1 to 3 times its mass of water; dilute surfactant A with 4 to 6 times its mass of water, and the water temperature is 80 to 95°C; dilute surfactant B with 4 to 6 times its mass diluted with water, the water temperature is 80-95°C;
[0073] Preparation of 2S coupling agent:
[0074] Add water with a total water content of 30% of the wetting agent into the container, sequentially add a pH regulator and a coupling agent, and stir to obtain a dispersion solution of the coupling agent;
[0075] Preparation of 3S sizing agent:
[0076] Add the diluted film-forming agent, surfactant A, and surfactant B obtained in step 1S to the coupling agent dispersion solution obtained in step 2S, supplement the water in the wetting agent formula, and stir evenly to obtain the product.
Embodiment 1
[0080] Weigh each component by mass percentage, and prepare the sizing agent according to the following steps:
[0081] 1S Dilution of film-forming agent, surfactant A and surfactant B: dilute the dimer acid modified epoxy resin emulsion with water 1 to 3 times its mass; dilute the acetylenic diol Germini nonionic surfactant with its Dilute with 4-6 times the mass of water, and the water temperature is 80-95°C; dilute the disemicarbazide polymer cationic surfactant with 4-6 times the mass of water, and the water temperature is 80-95°C;
[0082] Preparation of 2S coupling agent: add water with a total water content of 30% of the wetting agent into the container, add glacial acetic acid and A-151 in sequence, and stir to obtain a coupling agent dispersion solution;
[0083] Preparation of 3S sizing agent: add the diluted dimer acid-modified epoxy resin emulsion, acetylene glycol Germini nonionic surfactant, and diaminocarbamide polymer cationic surfactant prepared in step 1S to ...
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