Preparation method of alpha-silicon nitride powder
The technology of silicon nitride powder and powder is applied in the field of preparation of α-silicon nitride powder, which can solve problems such as affecting the formation of silicon nitride crystal grains, and achieve low production cost, high powder purity and easy control. Effect
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Embodiment 1
[0036] 1), Cr 2 o 3 Weigh the raw materials with Si powder according to the mass ratio of 2.5:97.5, and dope 2.5wt% Cr 2 o 3 The silicon powder of the powder is ball-milled, and the ball-milled powder is put into a silicon nitride ball mill tank, and silicon nitride balls and alcohol are added, wherein the powder: ball: alcohol mass ratio is 1:3:1.5. Put it into a planetary ball mill for ball milling, the rotating speed is 300r / min, and the ball milling time is 4h.
[0037] 2), the above ball milled doped 2.5wt% Cr 2 o 3 The silicon powder was suction filtered to remove the alcohol in the silicon powder; after that, the above filtered powder was dried in a vacuum drying oven to remove residual alcohol at a temperature of 40°C and a drying time of 4 hours. The above-mentioned vacuum-dried sample was ground and passed through a 40-mesh sieve to obtain a powder with uniform particles for subsequent nitriding experiments.
[0038] 3), the doped 2.5wt% Cr after above-mentione...
Embodiment 2
[0040] 1), Cr 2 o 3 Weigh the raw materials with Si powder according to the mass ratio of 2.5:97.5, and dope 2.5wt% Cr 2 o 3 The silicon powder of the powder is ball milled, and the ball milled powder is put into a silicon nitride ball mill tank, and silicon nitride balls and alcohol are added, wherein the powder: ball: alcohol mass ratio is 1:6:1.5. Put it into a planetary ball mill for ball milling, the rotating speed is 400r / min, and the ball milling time is 2h.
[0041]2), the above ball milled doped 2.5wt% Cr 2 o 3 The silicon powder was suction filtered to remove the alcohol in the silicon powder; after that, the above filtered powder was dried in a vacuum drying oven to remove residual alcohol at a temperature of 80°C and a drying time of 2 hours. The above-mentioned vacuum-dried sample was ground and passed through a 40-mesh sieve to obtain a powder with uniform particles for subsequent nitriding experiments.
[0042] 3), the doped 2.5wt% Cr after above-mentioned...
Embodiment 3
[0044] 1), Cr 2 o 3 Weigh the raw materials with Si powder according to the mass ratio of 2.5:97.5, and dope 2.5wt% Cr 2 o 3 The silicon powder of the powder is ball-milled, and the ball-milled powder is put into a silicon nitride ball mill tank, and silicon nitride balls and alcohol are added, wherein the powder: ball: alcohol mass ratio is 1:4:1.5. Put it into a planetary ball mill for ball milling, the rotating speed is 400r / min, and the ball milling time is 2h.
[0045] 2), the above ball milled doped 2.5wt% Cr 2 o 3 The silicon powder was suction filtered to remove the alcohol in the silicon powder; after that, the above filtered powder was dried in a vacuum drying oven to remove residual alcohol at a temperature of 80°C and a drying time of 2 hours. The above-mentioned vacuum-dried samples were ground and passed through a 70-mesh sieve to obtain a powder with uniform particles for subsequent nitriding experiments.
[0046] 3), the doped 2.5wt% Cr after above-mentio...
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