Double-layer infrared film glass with anti-reflection, self-cleaning and radiation cooling functions and preparation method thereof
A radiation cooling and self-cleaning technology, which is applied in the field of energy-saving building materials, can solve the problems of increasing infrared radiation and modulating infrared absorption, and achieves the effect of simple and efficient preparation method
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Embodiment 1
[0039] A method for preparing a double-layer infrared film material with anti-reflection, self-cleaning and radiation cooling functions, comprising the following steps:
[0040] a) Preparation of silica nanospheres:
[0041] Preparation of solution A: Mix the three according to the ratio of ammonia water: ethanol: water volume ratio of 3:16:24, and prepare an 8 mol / L solution.
[0042] Preparation of solution B: prepare ethyl orthosilicate solution according to the ratio of ethyl orthosilicate:ethanol volume ratio 1:23.
[0043]Solution A was mixed with solution B and stirred at room temperature for 2 h. After the reaction was completed, it was centrifuged and washed with ethanol to finally obtain silica nanospheres with a particle size of 200 nm.
[0044] b) Preparation of titania-coated silica core-shell structure:
[0045] Preparation of solution A: According to the mass ratio of silica nanospheres and hydroxypropyl cellulose of 1:1, introduce silica nanospheres and hydr...
Embodiment 2
[0055] A method for preparing a double-layer infrared film material with anti-reflection, self-cleaning and radiation cooling functions, comprising the following steps:
[0056] a) Preparation of silica nanospheres:
[0057] Preparation of solution A: Mix the three according to the ratio of ammonia water: ethanol: water volume ratio of 3:16:24, and prepare an 8 mol / L solution.
[0058] Preparation of solution B: prepare ethyl orthosilicate solution according to the ratio of ethyl orthosilicate:ethanol volume ratio 1:31.
[0059] Solution A was mixed with solution B and stirred at room temperature for 2 h. After the reaction was completed, it was centrifuged and washed with ethanol to finally obtain silica nanospheres with a particle size of 175 nm.
[0060] b) Preparation of titania-coated silica core-shell structure:
[0061] Preparation of solution A: According to the mass ratio of silica nanospheres and hydroxypropyl cellulose of 1:1, introduce silica nanospheres and hyd...
Embodiment 3
[0069] A method for preparing a double-layer infrared film material with anti-reflection, self-cleaning and radiation cooling functions, comprising the following steps:
[0070] a) Preparation of silica nanospheres:
[0071] Preparation of solution A: Mix the three according to the ratio of ammonia water: ethanol: water volume ratio of 3:16:24, and prepare an 8 mol / L solution.
[0072] Preparation of solution B: prepare ethyl orthosilicate solution according to the ratio of ethyl orthosilicate:ethanol volume ratio 1:46.
[0073] Solution A was mixed with solution B and stirred at room temperature for 2 h. After the reaction was completed, it was centrifuged and washed with ethanol to finally obtain silica nanospheres with a particle diameter of 150 nm.
[0074] b) Preparation of titania-coated silica core-shell structure:
[0075] Preparation of solution A: According to the mass ratio of silica nanospheres and hydroxypropyl cellulose of 1:1, introduce silica nanospheres and...
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