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Method of simultaneously improving uniformity of air flow and temperature in ion mobility pipe

A technology of ion transfer tube and ion mobility spectrometer, which is applied in the field of improving the uniformity of airflow and temperature in the ion transfer tube at the same time, and can solve the problems of increasing the manufacturing cost and volume of the whole migration spectrometer, it is difficult to ensure the cleanliness of the migration area, and there are no literature reports, etc. , to achieve the effect of improving the uniformity of airflow and temperature distribution, reducing turbulence and improving resolution

Inactive Publication Date: 2019-06-04
DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Reducing the flow velocity of the drift gas can reduce its influence on the temperature of the migration zone, and at the same time reduce the turbulence formed by the drift gas in the migration zone, but this method cannot completely solve the problem. In addition, when the drift gas velocity is too small , it is difficult to ensure the cleanliness of the migration area
The drift gas is heated to the same temperature as the transfer tube before entering the transfer tube, but this method requires additional heating and temperature control devices, which will increase the manufacturing cost and volume of the transfer spectrometer
The method to improve the uniformity of the airflow distribution in the migration area in the migration tube is generally to reduce the flow velocity of the drift gas to reduce its influence on the temperature of the migration area, but this method cannot completely solve the problem. In addition, when the drift gas velocity If the temperature is too small, it is difficult to ensure the cleanliness of the migration area
[0004] There is no literature report on the method of improving the uniformity of airflow distribution in the migration zone

Method used

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  • Method of simultaneously improving uniformity of air flow and temperature in ion mobility pipe
  • Method of simultaneously improving uniformity of air flow and temperature in ion mobility pipe
  • Method of simultaneously improving uniformity of air flow and temperature in ion mobility pipe

Examples

Experimental program
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Effect test

Embodiment 1

[0038]Simulate with fluent software: the drift flow rate is 200mL / min, the carrier gas flow rate is 10mL / min, and the heating temperature is 100°C. The internal air flow distribution diagram of the ion transfer tube without a circular metal plate, and the setting of two circles under the same conditions Airflow distribution diagram inside the ion transfer tube with a flat metal plate. Comparing the two image 3 As shown, it can be seen that the airflow distribution in the transfer zone in the transfer tube with two circular metal plates is more uniform, and there is basically no turbulent flow phenomenon.

Embodiment 2

[0040] Simulation with fluent software: the drift flow rate is 200mL / min, the carrier gas flow rate is 10mL / min, and the heating temperature is 100°C. The internal temperature distribution diagram of the ion transfer tube without a circular metal plate, and the setting of two circles under the same conditions Temperature distribution inside an ion transfer tube with a flat metal plate. Comparing the two Figure 4 As shown, it can be seen that the temperature distribution in the transfer region of the ion transfer tube with two circular metal plates is more uniform.

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Abstract

The invention relates to a method of simultaneously improving uniformity of an air flow and temperature in an ion mobility spectrometry mobility zone. After drift air of the ion mobility spectrometryenters a mobility pipe, the air sequentially flows through one or more than one drift air passing hole in a circular metal plate whose temperature is almost the same as that in the mobility zone and enters the mobility zone, the drift air is subjected to diversion and preheating through one or more than one drift air passing hole in the metal plate, the distribution uniformity of the air flow andthe flow velocity in the mobility zone can be improved simultaneously, and the resolution is thus improved.

Description

technical field [0001] The invention relates to a method for improving the uniformity of gas flow and temperature in a simultaneous ion transfer tube. Specifically, after the room temperature drift gas with a certain flow rate is passed into the ion transfer tube, it passes through one or more drift gas holes on the heated circular metal plate in turn, and then enters the migration area in the ion transfer tube, so as to achieve the effect of drift gas. The role of shunting and preheating can improve the uniformity of gas flow and temperature distribution in the ion transfer tube, thereby improving the resolution of the transfer spectrum. Background technique [0002] The uniformity of gas flow and temperature distribution in the ion transfer tube, especially in the transfer region, are two important factors affecting the resolution of the transfer spectrum. Conventional ion transfer tubes directly pass drift gas at room temperature into the transfer region, which will form...

Claims

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Application Information

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IPC IPC(8): G01N27/62H01J49/00
Inventor 李海洋陈红陈创厉梅蒋丹丹
Owner DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI
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