A kind of preparation method of formaldehyde purification material
A technology for formaldehyde purification and solid materials, applied in chemical instruments and methods, separation methods, molecular sieve catalysts, etc., can solve the problem of low formaldehyde purification rate and achieve the effect of ensuring adsorption
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[0023] (1) Crush amantadine into granules and put it into a beaker, add appropriate amount of ethylenediamine and water, and use an ultrasonic cell disruptor to sonicate it for 15 minutes, set the frequency to 20kHz, and the power to 900w. After ultrasonic treatment, place the beaker in the ice-water mixture, add the rotor after it cools down, and add appropriate amount of silica sol and H2PtCl4 solution dropwise under stirring state. After the dropwise addition, the beaker was stirred and heated to 90° C. and kept for 30 min to form a synthetic solution with a molar ratio of amantadine:silicon source:noble metal source:ethylenediamine:water of 47:100:10:400:11240.
[0024] (2) Add the pre-prepared DD3R molecular sieve particles (particle size: 300nm) to the synthesis solution at a mass ratio of 0.5% after ball milling, and place the synthesis solution in a microwave reactor, and under microwave conditions The hydrothermal synthesis was carried out under stirring for 72 hours ...
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