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Method for extracting lemon peel pectin through salt

A technology of lemon peel pectin and lemon peel, which is applied in the field of pectin preparation and extraction of lemon peel pectin through salt, can solve the problems of high cost, low yield of pectin, complicated process, etc., and prevent pectin from sealing and process Reasonable design and good extraction effect

Active Publication Date: 2019-03-08
广州市莱檬生物科技有限公司 +3
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For example, CN108794651A discloses a method for extracting pectin from the passion fruit peel, specifically discloses that after the passion fruit peel powder is dispersed in water, tartaric acid is added, heated and stirred for extraction, and the pectin extract is obtained after filtration. However, the pectin molecule of this technical scheme is It will be partially decomposed during the extraction process, the yield of pectin is low, and the extraction efficiency is poor
[0004] CN108892741A discloses a method for extracting peach pectin, which specifically discloses that the washed dried peach powder is added to an acetic acid solution for subcritical extraction, and after the extraction is completed, it is filtered to obtain a pectin extract without destroying the pectin structure. This technical solution has high cost and complex process, and is especially suitable for the extraction of pectin in peaches, so it cannot be popularized and applied on a large scale.
This method has high degree of gelation and high molecular weight of pectin, but the process is cumbersome and not suitable for industrial production
[0005] In summary, the prior art still lacks an efficient and low-cost pectin extraction process

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] A method for extracting lemon peel pectin by salt, comprising the following steps:

[0034] (1) Mixing: add 400kg of juiced lemon peel in a 10-ton tank, add 8 tons of water, and soak for 20 minutes;

[0035] (2) Organic acid treatment: In the case of constant stirring at a stirring speed of 500r / min, add citric acid to the system obtained in step (1), and control the temperature of the entire system to 60°C and pH to 3.0, and stir for 2 hours at the same time ;

[0036] (3) Salt extraction: also under the condition of constant stirring at a stirring speed of 500r / min, add 10kg of sodium citrate, 10kg of ammonium sulfate and 1kg of sodium tripolyphosphate mixed salt to the system obtained in step (2) , and control the temperature of the whole system to 80°C, while stirring for 2h;

[0037](4) Solid-liquid separation: solid-liquid separation by a horizontal screw centrifuge, the solid-liquid separation conditions are: the rotating speed is 3000-5000r / min, the time is 20...

Embodiment 2

[0040] A method for extracting lemon peel pectin by salt, comprising the following steps:

[0041] (1) Mixing: add 400kg of juiced lemon peel in a 10-ton tank, add 8 tons of water, and soak for 20 minutes;

[0042] (2) Organic acid treatment: In the case of constant stirring at a stirring speed of 500r / min, add citric acid to the system obtained in step (1), and control the temperature of the entire system to 60°C and pH to 3.0, and stir for 2 hours at the same time ;

[0043] (3) Salt extraction: also in the case of constant stirring at a stirring speed of 500r / min, add 10kg of sodium citrate, 15kg of ammonium sulfate and 1kg of sodium tripolyphosphate mixed salt to the system obtained in step (2) , and control the temperature of the whole system to 80°C, while stirring for 2h;

[0044] (4) Solid-liquid separation: solid-liquid separation by a horizontal screw centrifuge, the solid-liquid separation conditions are: the rotating speed is 3000-5000r / min, the time is 20min, th...

Embodiment 3

[0047] A method for extracting lemon peel pectin by salt, comprising the following steps:

[0048] (1) Mixing: add 400kg of juiced lemon peel in a 10-ton tank, add 8 tons of water, and soak for 20 minutes;

[0049] (2) Organic acid treatment: In the case of constant stirring at a stirring speed of 500r / min, add citric acid to the system obtained in step (1), and control the temperature of the entire system to 60°C and pH to 3.0, and stir for 2 hours at the same time ;

[0050] (3) Salt extraction: also in the case of constant stirring at a stirring speed of 500r / min, add 10kg of sodium citrate, 5kg of ammonium sulfate and 3kg of sodium tripolyphosphate mixed salt to the system obtained in step (2) , and control the temperature of the whole system to 80°C, while stirring for 2h;

[0051] (4) Solid-liquid separation: solid-liquid separation by a horizontal screw centrifuge, the solid-liquid separation conditions are: the rotating speed is 3000-5000r / min, the time is 20min, the...

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PUM

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Abstract

The invention discloses a method for extracting lemon peel pectin through salt. The method comprises the following steps: adding 400 to 500 kg of lemon peels into a 10-ton tank, adding water with 18 to 20 times of mass thereof and soaking for 15 to 30 min; adding organic acid under the constant-speed stirring situation and treating for 1 to 2 h; adding 20 to 30 kg of mixed salt under the constant-speed stirring situation and treating for 2 to 3 h; separating through centrifugal equipment to obtain liquid; vacuum concentrating the liquid through vacuum equipment and obtaining pectin concentrated liquid. According to the method disclosed by the invention, an acid method and a salt method are combined, so that not only are pectin molecules extracted in high efficiency, but also pectin molecules can keep integrity under the acid condition; organic acid and inorganic acid are mutually matched with each other, so that cellulose crystalline can be cracked more effectively, the pectin molecules can be more effectively dispersed from cell walls, the extracting efficiency is high, and the extracting effect is good.

Description

technical field [0001] The invention relates to the technical field of deep processing of agricultural products, in particular to a method for preparing pectin, in particular to a method for extracting lemon peel pectin with salt. Background technique [0002] Pectin is a natural polymer compound widely present in the cell wall and intercellular layer structure of higher plants. Therefore, the extraction of pectin requires the release of pectin from the cell wall of cellulose. At present, the traditional extraction process of pectin is the boiling water extraction method, which is to boil the extracted raw materials in water to dissolve the pectin, then centrifuge the pectin extract and filter to obtain the pectin clarified solution. This method can only extract part of the water-soluble pectin in the raw material, the yield is low, and the finished product contains various impurities. [0003] Some new pectin extraction methods have been developed in the prior art, mainly...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08B37/06
CPCC08B37/0048
Inventor 廖劲松
Owner 广州市莱檬生物科技有限公司
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