Method for removing tellurium from crude selenium slag
A crude selenium and primary technology, applied in the field of purification of crude selenium slag, can solve the problems of inability to produce qualified selenium products and high tellurium content of selenium products
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Embodiment 1
[0034] 1. Oxidation of crude selenium slag: add 30% hydrogen peroxide to tap water to dilute it into a 15% hydrogen peroxide solution, then add the hydrogen peroxide solution to the coarse selenium slag and stir. The tellurium content in the thick selenium slag is 1.57%. According to the reaction of the amount of tellurium contained in the thick selenium slag with the oxidizing agent, the ratio of the required oxidizing agent is calculated, and the concentration of 6% of the thick selenium slag weight is 15% hydrogen peroxide added to the crude selenium slag. In the selenium slag, stir it to make it mix evenly, and the oxidation reaction of tellurium occurs; then add NaOH to the solution for neutralization, and adjust the pH value to 5;
[0035] 2. The material after the oxidation reaction is melted: the material obtained in step 1 is added to the heating container, and heated to 260°C to melt it. After melting, the form of selenium remains unchanged, while the form of telluriu...
Embodiment 2
[0038] 1. Oxidation of crude selenium slag: add 30% hydrogen peroxide to tap water to dilute it into a 15% hydrogen peroxide solution, then add the hydrogen peroxide solution to the coarse selenium slag and stir. The tellurium content in the thick selenium slag is 1.57%. According to the reaction of the amount of tellurium contained in the thick selenium slag with the oxidizing agent, the ratio of the required oxidizing agent is calculated, and the concentration of 7% of the thick selenium slag weight is 15% hydrogen peroxide added to the crude selenium slag. In the selenium slag, stir it to make it mix evenly, and the oxidation reaction of tellurium occurs; then add KOH to the solution for neutralization, and adjust the pH value to 6;
[0039] 2. The material after the oxidation reaction is melted: the material obtained in step 1 is added to a heating container, and heated to 280°C to melt it. After melting, the form of selenium remains unchanged, while the form of tellurium c...
Embodiment 3
[0042]1. Oxidation of crude selenium slag: Add 30% hydrogen peroxide to tap water to dilute it into a 20% hydrogen peroxide solution, then add the hydrogen peroxide solution to the coarse selenium slag and stir. The tellurium content in the thick selenium slag is 1.57%. According to the reaction of the amount of tellurium contained in the thick selenium slag with the oxidizing agent, the ratio of the required oxidizing agent is calculated, and the concentration of 5% of the thick selenium slag weight is 20% hydrogen peroxide added to the crude selenium slag. In the selenium slag, stir it to make it mix evenly, and the oxidation reaction of tellurium occurs; then add NaOH to the solution for neutralization, and adjust the pH value to 6;
[0043] 2. The material after the oxidation reaction is melted: the material obtained in step 1 is added to the heating container, and heated to 240°C to melt it. After melting, the form of selenium remains unchanged, while the form of tellurium...
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