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Highly-efficient preparation method for dried orange peel absolute oil for flavoring of tobacco

A technology of tangerine peel and feeding port, which is applied in the application of cigarette flavoring, and the field of efficient preparation of tangerine peel pure oil, can solve the problems of insufficient extraction, reduced quality, long time consumption, etc., and achieves improvement of richness, aftertaste, production The effect of improving the rate and quality and reducing the production cost

Active Publication Date: 2019-01-29
CHINA TOBACCO YUNNAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These methods take a long time and are easy to destroy the aroma-causing ingredients in the orange peel. Because the orange peel contains a large amount of pectin, cellulose, etc., the flavonoids and volatile oils in the orange peel cannot be fully extracted, and the quality is reduced.
In addition, the existing tangerine peel extract is used in new tobacco products due to its complex composition, which affects the smoking experience of electronic cigarettes and heat-not-burn cigarettes

Method used

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  • Highly-efficient preparation method for dried orange peel absolute oil for flavoring of tobacco

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0068] The tangerine peel used for extracting raw materials adopts tangerine peel produced in Yunnan. The tangerine peel sample is dried, crushed to 20 mesh, and the feeding amount is 200kg. It is added in the ultrasonic extraction tank 1, the feeding port and the discharge port are sealed, and acetic acid of 5 times the weight of the tangerine peel sample is added. Methyl esters were ultrasonically extracted at 45°C for 35 minutes. After extraction, the air compressor was started to pressurize the ultrasonic extraction tank, allowing the extract to pass through the filter sieve plate at the outlet and lead to the chromatographic column for purification.

[0069] After the extract passed through the chromatographic column was transferred to the concentration tank, the temperature of the concentration tank was raised to 80° C., and at the same time, the vacuum pump was started to concentrate the extract until the methyl acetate was evaporated to dryness. Return the methyl acetat...

Embodiment 2

[0072]The tangerine peel absolute oil prepared by the above method is used in shredded cigarette tobacco, and the tangerine peel absolute oil is added to the shredded cigarette tobacco at a ratio of 5 / 100,000 of the weight of the shredded tobacco, and the shredded tobacco is made into finished cigarettes for evaluation and smoking. The results show that the tangerine peel absolute oil prepared by the present invention can effectively endow cigarettes with natural characteristic fragrance, increase the aroma quantity and aroma quality of cigarette smoking, and can also cover up the miscellaneous gases of cigarette smoking, improving the comfort of cigarette smoking properties, better than the control (i.e. the cigarette without adding the absolute oil of tangerine peel obtained by the present invention). or,

[0073] In the cigarette filter forming process, the tangerine peel absolute oil obtained by the present invention is added to triacetin by 1wt% of the amount of plasticiz...

Embodiment 3

[0076] During the preparation process of the electronic cigarette liquid, the tangerine peel absolute oil of the present invention is added to the orange peel flavored electronic cigarette liquid in a proportion of 5% by weight. The results show that: the total score of the dried tangerine peel absolute oil of the present invention is higher, and the advantages are mainly manifested in that the unique natural fragrance characteristics of dried tangerine peel are prominent, the aroma quality is good, and the amount of aroma is sufficient; In the same way (that is, the electronic cigarette that does not add the tangerine peel absolute oil that the present invention obtains).

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Abstract

The invention discloses a preparation method for dried orange peel absolute oil. The preparation method is performed with the following devices: an ultrasonic extraction tank (1), a chromatography column (2), an air compressor (3), a concentration tank (4), a reverse resin column (5), a condenser (6), a vacuum pump (8) and a solvent recovery tank (7). The preparation method comprises the followingsteps: 1, subjecting a dried orange peel raw material to ultrasonic extraction; 2, carrying out purification through the chromatography column (2); 3, carrying out concentration; 4, carrying out purification through the reverse resin column ( 5); and 5, carrying out decompressing to remove ethanol so as to obtain the dried orange peel absolute oil. The devices provided by the invention can realize highly-efficient extraction and purification of the dried orange peel absolute oil; and the dried orange peel absolute oil obtained by using the preparation method provided by the invention is usedin cigarettes, electronic cigarettes or heat-not-burn cigarettes, and effectively enhances and improves the suction comfort of the cigarettes, the electronic cigarettes and the heat-not-burn cigarettes.

Description

technical field [0001] The invention belongs to the field of preparation of essence and fragrance for tobacco, and in particular relates to a method for efficiently preparing tangerine peel absolute and the application of the tangerine peel absolute in flavoring cigarettes, electronic cigarettes and heat-not-burn cigarettes. Background technique [0002] Cigarette flavoring is the core technology to enhance the style of cigarettes. Especially in recent years, the continuous advancement of tobacco tar reduction and harm reduction has gradually reduced the amount of tar released in cigarettes, and the accompanying reduction in cigarette aroma and taste. This often requires the use of flavoring methods to ensure and improve the sensory quality of cigarettes, so as to satisfy consumers' pursuit of the aroma and taste of cigarettes. In addition, with the development of new tobacco products such as e-cigarettes and heat-not-burn cigarettes, there is also a strong demand for new ty...

Claims

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Application Information

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IPC IPC(8): C11B9/02
CPCC11B9/022C11B9/025C11B9/027
Inventor 高茜李雪梅管莹杨光宇巩效伟朱东来洪鎏刘春波申钦鹏张天栋凌军
Owner CHINA TOBACCO YUNNAN IND
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