A zif derived comoo 4 The preparation method of the electrode
A ZIF-67, Electrode Technology
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[0029] 1. Sample preparation
[0030] A ZIF-derived CoMoO 4 The preparation method of the electrode is to use high-temperature calcined ZIF-67 as a precursor, and prepare CoMoO by hydrothermal method 4 , the steps are: (1) take Na respectively 2 MoO4·2H 2 O and CoCl 2 ·6H 2 O was dissolved in deionized water, and stirred in a magnetic stirrer until dissolved; (II) adding the calcined powder of ZIF-67 at a temperature of 700 °C, and ultrasonically stirring until a homogeneous solution; (III) transferring the obtained solution to a reaction kettle , reacted at 160°C for 2h, and then cooled to room temperature; (IV) The obtained product was washed alternately with deionized water and absolute ethanol, then placed in a constant temperature drying oven at 60°C for 24h, taken out and ground to obtain the ZIF-67 derivative CoMoO 4 The product; (V) was soaked in acetone for 10 minutes, then added ethanol and washed for 10 minutes, and finally added 2mol / L hydrochloric acid for u...
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