Anti-ageing serum and preparing method thereof
A kind of essence and anti-aging technology, which is applied in the direction of pharmaceutical formulations, cosmetic preparations, dressing preparations, etc., can solve the problems of limited antioxidant capacity, ineffective effect, skin allergies, etc., achieve obvious wrinkle removal effect and restore skin Vitality, enhanced anti-aging effect
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Embodiment 1
[0024] An anti-aging essence, by weight percentage, said essence comprises the following raw materials:
[0025]
[0026] The plant extracts include sunflower seed extract, grape seed polyphenol and aloe extract.
[0027] The raw materials for the preparation of the fullerene derivatives include fullerene and azide-tripolyethylene glycol-carboxylic acid; the fullerene is dissolved in an organic solvent and added to the reactor, and the azide dissolved in the organic solvent is added thereto. Nitrogen-tripolyethylene glycol-carboxylic acid, heated to 60-90°C, heat preservation reaction for 24-72 hours, then add organic solvent, heat to 90-110°C, heat preservation reaction for 5-10 hours, spin evaporate the organic solvent, Obtain fullerene derivatives and black solid fullerenes that do not participate in the reaction, and silica gel column chromatography separates and purifies fullerenes to obtain carboxyl-containing fullerene derivatives, and the fullerenes are C 60 fuller...
Embodiment 2
[0038] On the basis of embodiment 1, present embodiment 2 is as a preferred embodiment of the present invention, a kind of anti-aging essence, and by weight percentage, described essence comprises following raw material:
[0039]
[0040] Wherein, in the preparation process of the fullerene derivative, the molar ratio of the fullerene to the azide-triethylene glycol-carboxylic acid is 1:10; the organic solvent is toluene and dioxygen According to the mixed solvent of six rings in the ratio of 20:80, heat to 80 ° C, heat preservation reaction for 48 hours, then add the mixed solvent, heat to 100 ° C, heat preservation reaction for 5-10 hours, rotary evaporate part of the organic solvent, add ether to The volume before the rotary evaporation, after continuing the rotary evaporation to remove the solvent, the fullerene derivatives and part of the black solid fullerenes that did not participate in the reaction were obtained, and the fullerenes were removed by silica gel column c...
Embodiment 3
[0043] On the basis of embodiment 2, present embodiment 3 is as a preferred embodiment of the present invention, a kind of anti-aging essence, and by weight percentage, described essence comprises following raw material:
[0044]
[0045]
[0046] Wherein, the molar ratio of the fullerene to the azide-triethylene glycol-carboxylic acid is 1:12; the preparation process of the fullerene derivative is the same as in Example 2, and the preparation of the essence Method is with embodiment 1.
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