Preparation method of efficient composite alcohol-based fuel

A technology for compound alcohol and fuel, which is applied in the direction of fuel, liquid carbon-containing fuel, petroleum industry, etc., can solve the problems of waste, high fuel loss, human health impact, etc., and achieve high fuel utilization rate, reduced fuel evaporation rate, and combustion effect. Good results

Active Publication Date: 2018-12-07
ANHUI SHENGBAO NEW ENERGY TECH CO LTD
View PDF4 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In alcohol-based fuels, during the combustion process of methanol, due to its very low boiling point, direct combustion will cause part of the methanol to gasify, resulting in a large amount of waste, and the loss of fuel is very high
Moreover, if methanol vapor is inhaled by the human body in large quantities, it will also have an impact on human health.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0015] Step 1. Add 50 parts by mass of methanol, 6.7 parts by mass of concentrated sulfuric acid with a mass fraction of 98%, and levulinic acid of 120 parts by mass in the reaction kettle with a condensation recovery device. Reaction at 70°C for 6h. The yield of methyl levulinate was 63.3%.

[0016] Step 2, dehydrating the product inside the reactor with water-absorbent resin to obtain a mixed solution, then adding anhydrous barium chloride to the mixed solution and stirring to generate a mixture containing precipitation, the mass ratio of the mixed solution to anhydrous barium chloride is 15:6; the mixture containing the precipitate was filtered with filter paper to remove the precipitate to obtain a premix, which contained methyl levulinate and methanol.

[0017] Step 3, mixing and stirring the premix and veratrole according to the mass ratio of 100:26 to obtain the finished product.

Embodiment 2

[0019] Step 1. Add 500 parts by mass of methanol, 8.9 parts by mass of concentrated sulfuric acid with a mass fraction of 98%, and levulinic acid of 120 parts by mass in the reaction kettle with a condensation recovery device. Reaction at 70°C for 7h. The yield of methyl levulinate was 64.1%.

[0020] Step 2, dehydrating the product inside the reactor with water-absorbent resin to obtain a mixed solution, then adding anhydrous barium chloride to the mixed solution and stirring to generate a mixture containing precipitation, the mass ratio of the mixed solution to anhydrous barium chloride is 70:7; the mixture containing the precipitate is filtered with filter paper to remove the precipitate to obtain a premix, which contains methyl levulinate and methanol;

[0021] Step 3, mixing and stirring the premix and veratrole according to the mass ratio of 100:28 to obtain the finished product.

Embodiment 3

[0023] Step 1. Add 1170 parts by mass of methanol, 9.8 parts by mass of concentrated sulfuric acid with a mass fraction of 98%, and levulinic acid of 120 parts by mass in the reaction kettle with a condensation recovery device, and heat the materials in the reaction kettle to 65 ~ Reaction at 70°C for 8h. The yield of methyl levulinate was 63.7%.

[0024] Step 2, dehydrating the product inside the reactor with water-absorbent resin to obtain a mixed solution, then adding anhydrous barium chloride to the mixed solution and stirring to generate a mixture containing precipitation, the mass ratio of the mixed solution to anhydrous barium chloride is 130:7.5; the mixture containing the precipitate was filtered with a filter paper to remove the precipitate to obtain a premix, which contained methyl levulinate and methanol.

[0025] Step 3, mixing and stirring the premix and veratrole according to the mass ratio of 100:29 to obtain the finished product.

[0026] Combustion Loss Exp...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention relates to a preparation method of efficient composite alcohol-based fuel. Methanol, concentrated sulfuric acid and levulinic acid are sequentially added to a reaction vessel with a condensation recovery device, and the materials in the reaction vessel are heated to 65-70 DEG C for reaction for 6-8 h; products in the reaction vessel are performed an impurity removing process to obtain a premixture containing methyl levulinate and methanol; and the premixture and veratrole are mixed and uniformly stirred to prepare the finished product. The preparation method uses the levulinic acid and methanol to be converted into and synthesize the methyl levulinate, then optimizes the impurity removing process of the methyl levulinate, and so the impurity removing process of the methyl levulinate can be achieved without rectification. Compared with a fuel evaporation rate of direct combustion of methanol, the fuel evaporation rate of the composite alcohol-based fuel of the invention isreduced by 67%. Therefore, the fuel utilization rate is high, and the combustion effect is good.

Description

technical field [0001] The invention relates to the technical field of alcohol-based fuels, in particular to a preparation method of high-efficiency composite alcohol-based fuels. Background technique [0002] Alcohol-based fuel is a fuel mainly composed of alcohols (such as methanol, ethanol, butanol, etc.). The combustion value of biofuel is lower than that of liquefied petroleum gas and diesel, but the price is more advantageous. It can be used as an alternative fuel for petroleum liquefied petroleum gas and fuel diesel. It is low-cost, safe and convenient. It has no residue residue, no black bottom, and is clean, hygienic and safe , cheap, easy to buy raw materials, easy to use, etc., the cost is only about one-third of the wholesale price of petroleum liquefied gas or diesel, huge profit margins, and extremely high investment value. [0003] As an important platform compound in the process of biomass conversion, methyl levulinate is widely used as food additives, spice...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C10L1/02C10L1/19C10L1/185
CPCC10L1/02C10L1/18C10L1/1852C10L1/19C10L2230/22
Inventor 曹大强
Owner ANHUI SHENGBAO NEW ENERGY TECH CO LTD
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap