Antibacterial and anti-radiation pure silk fabric and preparation method thereof
A real silk and anti-radiation technology, applied in the field of textile weaving, can solve the problems of easy wrinkling of silk fabrics, limit the development of silk fabrics, and easy yellowing, etc., and achieve good anti-radiation performance, strong antibacterial properties, strong moisture absorption and breathability Effect
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Embodiment 1
[0032] The components of the raw materials of the finishing solution are: 7.5 parts of silkworm pupa chitosan, 2 parts of citric acid, 3.5 parts of alkylamide betaine, 3 parts of morning glory extract, 3.2 parts of wood sorrel extract, and dioctyl sulfosuccinate 1.5 parts of sodium ester;
[0033] Preparation of modified resin cotton: Take 40 parts of resin cotton washed with acetone, ethanol and deionized water and then dried at 55℃ to remove impurities in the resin cotton to obtain dried resin cotton; take maleic two 30 parts of acid anhydride, 18 parts of polyethylene glycol, and 9 parts of 1,2,3,4-butanetetracarboxylic acid are placed in the reaction kettle, and then dried resin cotton is added for immersion grafting for 2h, and then plasma irradiation , Set the irradiation time to 4.5min, and wash the grafted resin cotton after plasma irradiation with deionized water at 78℃ for 60min, and then repeat the washing with clean deionized water to completely remove the monomer att...
Embodiment 2
[0039] The components of the raw materials of the finishing solution are: 6 parts of silkworm pupa chitosan, 1.5 parts of citric acid, 5 parts of alkylamide betaine, 4 parts of morning glory extract, 3.5 parts of wood sorrel extract, dioctyl sulfosuccinate 1.8 parts of ester sodium salt;
[0040] Preparation of modified resin cotton: Take 42 parts of resin cotton washed with acetone, ethanol and deionized water and then dried at 60℃ to remove impurities in resin cotton to obtain dried resin cotton; take maleic two 38 parts of acid anhydride, 16 parts of polyethylene glycol, and 10 parts of 1,2,3,4-butanetetracarboxylic acid are placed in the reaction kettle, and then dried resin cotton is added for dipping and grafting for 1.9h, and then plasma Irradiate, set the irradiation time to 5min, and wash the grafted resin cotton after plasma irradiation with deionized water at 80℃ for 52min, and then repeat the washing with clean deionized water to completely remove the monomer attached...
Embodiment 3
[0046] The ingredients of the finishing solution are 8 parts of silkworm chitosan, 1 part of citric acid, 3 parts of alkylamide betaine, 5 parts of morning glory extract, 4 parts of wood sorrel extract, and dioctyl sulfosuccinate 1 part of sodium ester;
[0047] Preparation of modified resin cotton: Take 50 parts of resin cotton washed with acetone, ethanol and deionized water and then dried at 58℃ to remove impurities in resin cotton to obtain dried resin cotton; take maleic two 35 parts of acid anhydride, 16 parts of polyethylene glycol, 8.5 parts of 1,2,3,4-butanetetracarboxylic acid are placed in the reactor, and then the dried resin cotton is added for immersion grafting for 1.8h, and then plasma Irradiate, set the irradiation time to 3.5min, and wash the grafted resin cotton after plasma irradiation with deionized water at 75℃ for 50min, and then repeat the shaking and washing with clean deionized water to completely remove the monomer attached to its surface. Then put the...
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