Preparation method of graphene/silicon carbide/aluminum composite material
A technology of aluminum composite materials and graphene, which is applied in the field of metal matrix composite materials, can solve the problem of low thermal conductivity of composite materials, achieve uniform and dense structure, and inhibit thermal expansion
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Embodiment 1
[0021] Silicon carbide fibers (100nm in diameter, 50μm in length) and graphene oxide (10μm in diameter, 2nm in thickness) were ultrasonically dispersed in ethanol solution at a ratio of 1:9 (v:v) for 1h, and configured into 3 mg / ml dispersion, then transferred to a PTPE mold (mold size 16×16×3cm), the mold was placed on the surface of liquid nitrogen for 10 minutes, directional and orderly frozen from top to bottom, and then the sample was freeze-dried, dried The time is 48 hours, and the silicon carbide fiber / three-dimensional graphene skeleton with an oriented and ordered network structure is obtained; after that, pre-sintering is carried out in a tube furnace, and the temperature is raised to 800 degrees Celsius at a speed of 20 degrees Celsius / min, and the temperature is kept for 6 hours to obtain a solidified Silicon carbide fiber / three-dimensional graphene skeleton with oriented and ordered network structure; placing a sufficient amount of aluminum block on silicon carbid...
Embodiment 2
[0023] Silicon carbide fibers (200nm in diameter, 50μm in length) and graphene oxide (20μm in diameter, 2nm in thickness) were ultrasonically dispersed in ethanol solution at a ratio of 1:9 (v:v) for 1h, and configured into 3 mg / ml dispersion, then transferred to a PTPE mold (mold size 16×16×3cm), the mold was placed on the surface of liquid nitrogen for 10 minutes, directional and orderly frozen from top to bottom, and then the sample was freeze-dried, dried The time is 48 hours, and the silicon carbide fiber / three-dimensional graphene skeleton with an oriented and ordered network structure is obtained; after that, pre-sintering is carried out in a tube furnace, and the temperature is raised to 800 degrees Celsius at a speed of 20 degrees Celsius / min, and the temperature is kept for 6 hours to obtain a solidified Silicon carbide fiber / three-dimensional graphene skeleton with oriented and ordered network structure; placing a sufficient amount of aluminum block on silicon carbid...
Embodiment 3
[0025] Silicon carbide fibers (100nm in diameter, 50μm in length) and graphene oxide (10μm in diameter, 2nm in thickness) were ultrasonically dispersed in an ethanol solution at a ratio of 1:9 (v:v) for 1h, and configured into 10mg / ml dispersion, then transferred to a PTPE mold (mold size 16×16×3cm), the mold was placed on the surface of liquid nitrogen for 10 minutes, directional and orderly frozen from top to bottom, and then the sample was freeze-dried, drying time After 48 hours, the silicon carbide fiber / three-dimensional graphene skeleton with an oriented and ordered network structure is obtained; after that, pre-sintering is carried out in a tube furnace, and the temperature is raised to 800°C at a speed of 20°C / min, and the temperature is kept for 6h to obtain a solidified orientation. The silicon carbide fiber / three-dimensional graphene skeleton of the network structure arranged in an orderly manner; After placing a sufficient amount of aluminum block on the silicon c...
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