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Method for testing pore closing temperature of diaphragm

A closed-cell temperature and test method technology, applied in thermometers, thermometer applications, measuring devices, etc., can solve the problems of test result influence, resistance increase, electrolyte volatilization and decomposition, etc., to achieve simple and reliable test methods, accurate measurement, The effect of high data accuracy

Active Publication Date: 2018-07-20
HEFEI GUOXUAN HIGH TECH POWER ENERGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These test methods are to heat the diaphragm after adding the electrolyte. Because the closed cell temperature of the diaphragm is about 130°C-150°C, the electrolyte will volatilize and decompose during the process of heating to the target temperature. It will cause the resistance to increase, which will have a great impact on the test results

Method used

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  • Method for testing pore closing temperature of diaphragm
  • Method for testing pore closing temperature of diaphragm
  • Method for testing pore closing temperature of diaphragm

Examples

Experimental program
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Effect test

Embodiment

[0042] Heat the 12-micron PE base film at different temperatures of 120°C, 130°C, and 140°C to obtain diaphragms treated at different temperatures, and then use a knife die to punch the diaphragm into several square sheets of 41mm×30mm. Paste the green glue on the dust-free paper, punch it into several square sheets of 50mm×32mm with a die cutter, and punch a round hole with a diameter of 12mm in the middle with a puncher; peel the green glue from the dust-free paper Open, paste the diaphragms treated at different temperatures on the green glue, and paste 1 layer, 2 layers, 3 layers, 4 layers, and 5 layers respectively. Punch 8 micron thick copper foil into several square sheets of 39mm×28mm with a knife die; punch 86 micron thick aluminum-plastic film into several square sheets of 60mm×80mm with a knife die; according to the order from top to bottom The sequence of standard aluminum-plastic film, standard copper foil, separator, standard copper foil, and standard aluminum-pla...

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Abstract

The invention discloses a method for testing the pore closing temperature of a diaphragm. The method comprises the following steps: preparing a first standard diaphragm, a second standard diaphragm, athird standard diaphragm, standard green adhesive tapes, a standard copper foil and a standard aluminum-plastic film, wherein the middle of the standard green plastic adhesive is provided with a circular hole with a preset diameter; respectively pasting one to five layers of the first standard diaphragm to one of the standard green adhesive tapes to obtain a first target diaphragm; respectively pasting one to five second standard diaphragms to one of the standard green adhesive tapes to obtain a second target diaphragm; respectively pasting one to five layers of the third standard diaphragm to one of the standard green adhesive tapes to obtain a third target diaphragm; sequentially assembling the first target diaphragm, the second target diaphragm, the third target diaphragm, the standardcopper foil, the standard aluminum-plastic film and a preset battery to obtain a corresponding flexibly packed battery; and measuring impedance of the flexibly packed battery by adopting an electrochemical workstation, linearly fitting the ohmic impedance value and the diaphragm layer number, and calculating the ion conductivity of the diaphragm to obtain the catastrophe point of the ion conductivity of the diaphragm, that is the corresponding pore closing temperature of the diaphragm.

Description

technical field [0001] The invention relates to the technical field of diaphragm closed cell temperature testing, in particular to a diaphragm closed cell temperature test method. Background technique [0002] Lithium-ion batteries have the advantages of high specific energy, high working voltage, no memory effect, long cycle life, and less environmental pollution. With the widespread application of lithium-ion batteries, the safety of batteries has received more and more attention. At present, the safety of lithium-ion batteries is still one of the key issues hindering their large-scale application in electric vehicles, energy storage and other fields. In unexpected situations, lithium-ion batteries may catch fire and explode, causing great personal injury and property loss. [0003] The battery is mainly composed of positive electrode material, negative electrode material, electrolyte and separator. The separator is an important part of the battery. The separator is main...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N25/12G01R27/02G01K13/00
CPCG01K13/00G01N25/12G01R27/02
Inventor 鲁扬张峥
Owner HEFEI GUOXUAN HIGH TECH POWER ENERGY
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