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Preparation method of herba artemisiae selengensis enzymolysis extract and application of herba artemisiae selengensis enzymolysis extract to cigarette

A kind of technology of extract and wormwood enzyme, which is applied in the field of preparation of wormwood enzymatic hydrolysis extract, can solve the problems of rare extraction of flavors and fragrances, achieve the effect of improving aroma quality and aroma richness, delicate smoke, and increasing extraction efficiency

Active Publication Date: 2018-07-10
CHINA TOBACCO JIANGXI IND CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] At present, wormwood is mainly edible, and there are studies using wormwood to prepare fruit and vegetable beverages, such as: a wormwood vinegar drink and its preparation method (patent number 201611227127.2), but it is rare to use it as a substrate to extract flavors and fragrances, especially tobacco flavor

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] A method for preparing an enzymatic hydrolysis extract of Artemisia arborescens, comprising the steps of:

[0034] (1) Pretreatment: Wash the wild Artemisia spp., which is a special product along the coast of Poyang Lake in Jiangxi, separate the leaves and stalks, and cut the stalks into sections for later use;

[0035] (2) Extraction by steam distillation: put 100g of wormwood leaves in a round bottom flask, add 600g of water until the leaves are submerged, add 0.2g of compound enzyme solution A, soak for 12 hours, add a small amount of zeolite, and steam distill to Stop the extraction when the increase rate of the oil precipitated in the volatile oil extractor slows down significantly, and after collecting the oil, dilute the oil 10 times with absolute ethanol to obtain extract A;

[0036] (3) Enzymatic hydrolysis and extraction: take 100g of Artemisia stalks and place them in a 2.5L flask, add 500g of deionized water and 0.2g of compound enzyme solution B, stir, cont...

Embodiment 2

[0043] A method for preparing an enzymatic hydrolysis extract of Artemisia arborescens, comprising the steps of:

[0044] (1) Pretreatment: Wash the wild Artemisia spp., which is a special product along the coast of Poyang Lake in Jiangxi, separate the leaves and stalks, and cut the stalks into sections for later use;

[0045] (2) Extraction by steam distillation: put 100g of wormwood leaves in a round bottom flask, add 600g of water until the leaves are submerged, add 0.2g of compound enzyme solution A, soak for 12 hours, add a small amount of zeolite, and steam distill to Stop the extraction when the increase rate of the oil precipitated in the volatile oil extractor slows down significantly, and after collecting the oil, dilute the oil 20 times with absolute ethanol to obtain extract A;

[0046] (3) Enzymatic extraction: Take 100g of Artemisia stalks and place them in a 2.5L flask, add 600g of deionized water and 0.2g of compound enzyme solution B, stir, control the heating t...

Embodiment 3

[0053] A method for preparing an enzymatic hydrolysis extract of Artemisia arborescens, comprising the steps of:

[0054] (1) Pretreatment: Wash the wild Artemisia spp., which is a special product along the coast of Poyang Lake in Jiangxi, separate the leaves and stalks, and cut the stalks into sections for later use;

[0055] (2) Extraction by steam distillation: put 100g of wormwood leaves in a round bottom flask, add 600g of water until the leaves are submerged, add 0.2g of compound enzyme solution A, soak for 12 hours, add a small amount of zeolite, and steam distill to Stop the extraction when the increase rate of the oil precipitated in the volatile oil extractor slows down significantly, and after collecting the oil, dilute the oil 30 times with absolute ethanol to obtain extract A;

[0056] (3) Enzymatic hydrolysis and extraction: take 100g of Artemisia argyi stalks and place them in a 2.5L flask, add 700g of deionized water and 0.2g of compound enzyme solution B, stir...

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PUM

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Abstract

The invention discloses a preparation method of a herba artemisiae selengensis enzymolysis extract. The method comprises the following steps of (1) performing pretreatment; (2) extracting folium artemisiae selengensis treated by a composite enzymolysis solution A by a water steam distillation method to obtain an extract A; (3) performing enzymolysis extraction on the rhizome artemisiae selengensisby using the composite enzymolysis solution B; (4) performing alcohol extraction: performing alcohol extraction over the night on the rhizome artemisiae selengensis enzymolysis extract; (5) performing suction filtration concentration to obtain an extract B; (6) performing compounding: uniformly mixing the extract A and the extract B according to the proportion; adding 1,2-propanediol accounting for 20 percent of the total mass of the extract A and the extract B; performing uniform mixing to obtain the herba artemisiae selengensis enzymolysis extract. The enzymolysis method is used for respectively treating the folium artemisiae selengensis and the rhizome artemisiae selengensis; the natural raw materials are sufficiently utilized; the effects of improving the extraction efficiency and improving the fragrance quality of the herba artemisiae selengensis extracts can be achieved; through a compounding process, the fragrance characteristics of the herba artemisiae selengensis are preferably optimized; when the prepared herba artemisiae selengensis enzymolysis extract is applied to cigarettes, the cigarette fragrance substances and the fragrance richness can be effectively improved, sothat the smoke gas is fine and adequate.

Description

technical field [0001] The invention relates to the technical field of tobacco spices, in particular to a preparation method of an enzymatic hydrolysis extract of Artemisia argyi and its application in cigarettes. Background technique [0002] In the existing technology, the core competitiveness of "Chinese-style cigarettes" is to form a characteristic style of products, embody individuality and differentiation, and adapt to the smoking habits and consumption needs of Chinese consumers. Flavors and fragrances for Chinese-style cigarettes are the "soul" of Chinese-style cigarette products and the mystery of the formation of the style and characteristics of "Chinese-style cigarettes". Scientifically adding flavors and ingredients to cigarettes is an important means to highlight the individual style of cigarette products. To improve and enhance the smoke concentration and aroma, currently only by means of flavoring technology. [0003] Constructing flavors and fragrances and ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24B15/30
CPCA24B15/307C11B9/00
Inventor 徐达苏加坤张晓旭蔡继宝郭磊陈若星罗娟敏邵灯寅
Owner CHINA TOBACCO JIANGXI IND CO LTD
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