Magnesium alloy surface blue self pore sealing ceramic layer and preparation method
A technology of ceramic layer and magnesium alloy, applied in the field of preparation of blue micro-arc oxidation ceramic layer, can solve the problem of less development work of blue micro-arc oxidation ceramic layer on magnesium surface, and achieve excellent corrosion resistance and mechanical properties, corrosion resistance Excellent physical and mechanical properties, and the effect of enhancing protective performance
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Embodiment 1
[0029] In this embodiment, the blue self-sealing hole micro-arc oxidation ceramic layer on the surface of the magnesium alloy, that is, after adding a certain amount of K 2 TiF 6 The micro-arc oxidation ceramic layer was prepared in the electrolyte, so that a ceramic layer doped with Ti element was formed in situ on the surface of the magnesium alloy substrate, and the thickness was 10 μm.
[0030] The preparation method of the magnesium alloy blue self-sealing micro-arc oxidation ceramic layer includes the following steps:
[0031] Step 1: After degreasing and degreasing the wire-cut magnesium alloy sample, it is ground with different water sandpaper, and then washed with water after polishing to prepare for micro-arc oxidation treatment.
[0032] Step 2: Prepare the silicate-based micro-arc oxidation electrolyte according to the matching principle of the micro-arc oxidation electrolyte, where K 2 TiF 6 The concentration is 3.5 g / L;
[0033] Step 3: Use a DC pulse micro-a...
Embodiment 2
[0036] In this embodiment, the blue self-sealing hole micro-arc oxidation ceramic layer on the surface of the magnesium alloy, that is, after adding a certain amount of K 2 TiF 6 A micro-arc oxidation ceramic layer was prepared in the electrolyte, so that a magnesium oxide porous film doped with Ti was formed on the surface of the magnesium alloy substrate in situ, and the thickness of the ceramic layer was 10 μm.
[0037] The preparation method of the magnesium alloy blue self-sealing micro-arc oxidation ceramic layer includes the following steps:
[0038] Step 1: After degreasing and degreasing the wire-cut magnesium alloy sample, it is ground with different water sandpaper, and then washed with water after polishing to prepare for micro-arc oxidation treatment.
[0039] Step 2: Prepare the silicate-based micro-arc oxidation electrolyte according to the matching principle of the micro-arc oxidation electrolyte, where K 2 TiF 6 The concentration is 5 g / L;
[0040] Step 3:...
Embodiment 3
[0043] In this embodiment, the blue self-sealing hole micro-arc oxidation ceramic layer on the surface of the magnesium alloy, that is, after adding a certain amount of K 2 TiF 6 The micro-arc oxidation ceramic layer was prepared in the electrolyte, so that a ceramic layer doped with Ti element was formed in situ on the surface of the magnesium alloy substrate, and the thickness was 10 μm.
[0044] The preparation method of the magnesium alloy blue self-sealing micro-arc oxidation ceramic layer includes the following steps:
[0045] Step 1: After degreasing and degreasing the wire-cut magnesium alloy sample, it is ground with different water sandpaper, and then washed with water after polishing to prepare for micro-arc oxidation treatment.
[0046] Step 2: Prepare the silicate-based micro-arc oxidation electrolyte according to the matching principle of the micro-arc oxidation electrolyte, where K 2 TiF 6 The concentration is 10 g / L;
[0047] Step 3: Use a DC pulse micro-ar...
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