Method for preparing basic magnesium borate whiskers by using bitter halogen of salt lakes
A technology of magnesium borate whiskers and bittern, which is applied in the field of preparing basic magnesium borate whiskers, can solve the problems of consuming manpower and material resources, affecting the ecological balance of offshore waters, and insufficient utilization of bittern, and achieves the effect of reducing manpower
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[0040] The method of utilizing salt lake bittern to prepare basic magnesium borate whiskers of the present embodiment may further comprise the steps:
[0041] S1. prepare basic magnesium borate whisker, and record data,
[0042] (1) Take 500 mL of bittern from Chaerhan Salt Lake, filter and discard the insoluble matter; the magnesium ion concentration is measured to be 2.63 mol / L;
[0043] (2) Prepare 0.900mol / L Na 2 B 4 o 7 the solution
[0044] (3) Add Na to bittern 2 CO 3 -NaHCO 3 Buffer volume 8mL, pH=(9.2±0.3). ;
[0045] (4) Take 100mL of the above-mentioned bittern solution, put it in a 1.00L beaker, and then slowly add Na 2 B 4 o 7 After adding 80 mL of the solution, put the mixed system in a water bath with a water temperature of 40°C to continue aging for 54 hours to obtain the basic magnesium borate whisker precursor;
[0046] (5) Put the generated basic magnesium borate whisker precursor into a hydrothermal reaction kettle, set the hydrothermal reaction...
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