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Method for determining content of nitidine chloride in radix zanthoxyli toothpaste

A technology of chlorinating alkaloids and alkaloids, which is applied in the field of chemical detection and can solve problems such as unfavorable product quality control

Inactive Publication Date: 2018-05-11
WUZHOU INST FOR FOOD & DRUG CONTROL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] According to the "Effective Toothpaste QB / T 2966-2014", the functional toothpaste should be qualitatively or quantitatively determined according to the relevant standards. (Tianqi) Determination of saponin content, determination of effective components of Corydalis praecox, xylitol content, etc. to detect the functional components, and some scholars have also tested the total flavonoid glycosides, jiulixiangone, sinomenine, corydalin, and pomelo peel in toothpaste. Determination of the content of glucoside and puerarin [1-4] , but as a functional toothpaste, there is no detection method for Liangmianzhen toothpaste, which is not conducive to product quality control

Method used

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  • Method for determining content of nitidine chloride in radix zanthoxyli toothpaste
  • Method for determining content of nitidine chloride in radix zanthoxyli toothpaste
  • Method for determining content of nitidine chloride in radix zanthoxyli toothpaste

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Embodiment 1

[0028] 1. Instruments and reagents

[0029] 1.1 Instrument

[0030] Agilent 1260 bio-inert quaternary liquid chromatograph;

[0031] Agilent ZORBAX SB-C18 chromatographic column (4.6mm×250mm, 5μm);

[0032] German IKA C-MAG HS 7 heating magnetic stirrer;

[0033] American Beckman company AllegraX-15R high-performance general-purpose desktop centrifuge;

[0034] German Sigma 3K15 desktop refrigerated centrifuge;

[0035] Sartorius Scientific Instruments (Beijing) Co., Ltd. Quintix224-1CN electronic balance; accuracy 0.1mg;

[0036] Diaphragm vacuum pump GM-0.33.

[0037] 1.2 Reagent

[0038] Chlorinated ampoules reference substance; content (National Institute for Food and Drug Control, batch number: 110848-200502);

[0039] Liangmianzhen toothpaste samples (Liuzhou Liangmianzhen Co., Ltd., product batch numbers: B20190216A1, G20190524B1, F20190612B1, the methodology used in this article is the product batch number is B20190216A1 samples);

[0040] Negative toothpaste s...

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Abstract

The invention discloses a method for determining the content of nitidine chloride in radix zanthoxyli toothpaste, and belongs to the field of chemical detection. The method is accurate, simple and convenient and can be used for controlling the content of nitidine chloride in the radix zanthoxyli toothpaste. The method comprises the following sub-steps sequentially: firstly, extracting nitidine chloride from radix zanthoxyli with ethanol, and collecting ethanol extract; secondly, determining the content of nitidine chloride in the ethanol extract with HPLC (high performance liquid chromatography). The method can be used for determining the content of nitidine chloride in the radix zanthoxyli toothpaste.

Description

technical field [0001] The invention belongs to the field of chemical detection, in particular to a method for measuring the content of lianthine chloride in liangmianzhen toothpaste. Background technique [0002] ZanthorμLumnitidum (Roxb.) DC. Bitter, pungent, neutral in nature, slightly toxic, returns to Liver and Stomach Meridians. It has the effects of promoting qi and relieving pain, promoting blood circulation and removing blood stasis, dispelling wind and dredging collaterals, and is used for bruises, rheumatic arthralgia, stomach pain, and toothache caused by qi stagnation and blood stasis. The main active ingredient of LMZ is LMZ chloride, and now LMZ is also widely used in Chinese patent medicines, such as Fufang Fengshining Capsules and Fuyanjing Tablets. Clinical trials have shown that adding double-sided needles to toothpaste can relieve toothache, relieve inflammation, reduce dental plaque and gingivitis, and help prevent gum bleeding and gum recession and ot...

Claims

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Application Information

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IPC IPC(8): G01N30/06G01N30/74
Inventor 张云平黄林杰赖秀梅
Owner WUZHOU INST FOR FOOD & DRUG CONTROL
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