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Energy-saving low-pressure extraction cold melamine production process

A technology for extracting and cooling melamine and melamine, which is applied in the field of energy-saving low-pressure extraction and cooling of melamine production technology, can solve the problems of compressor impeller scarring, low product quality rate, limited promotion and application, etc., and achieves remarkable energy-saving effect and stable products. Quality, the effect of extending the operating cycle

Active Publication Date: 2021-07-09
王庆锋
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  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The main shortcoming of the low-pressure melamine process unit lies in the short operation period and high power consumption. The main problems of the unit are: hot gas cooler heat exchange pipe blockage; crystallizer wall collapse blocks the discharge port; compressor impeller scarring ; Low product rate and high consumption (urea, electricity, catalyst, etc.)
The high-pressure melamine production process needs to pay high patent fees and large investment, which limits its popularization and application

Method used

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  • Energy-saving low-pressure extraction cold melamine production process

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Embodiment 1

[0029] A melamine plant of 50,000 tons / year has been built with the method of the present invention, and the investment is less than 215 million yuan; 2 years of operation and trial production, the average daily production of 180 tons of melamine; the rate of excellent product quality reaches 96.78%; each unit consumption index: electricity ≤700 kWh; urea ≤3.0 tons; catalyst ≤1 kg; continuous operation period up to 180 days, with an average of 145 days; all emission indicators are within the allowable range of environmental protection indicators.

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Abstract

The invention provides an energy-saving low-pressure extraction and cooling melamine production process, including a melamine reactor, a hot air cooler, a filter, a crystallizer, a trap, a carrier gas compressor, a cold air fan, a urine scrubber, a carrier gas heater, etc. . The upper part of the crystallizer has a double-layer cold air ring pipe, and the lower part of the crystallizer has a rotary scraper; the air intake of the carrier gas compressor and the air-conditioning fan are separated, the air intake of the air-conditioning compressor adopts hot process air, and the air intake of the air-conditioning fan adopts cold process air; From the outlet of the carrier gas preheater, a hot process gas is led out to distribute hot ammonia gas or superheated steam into the hot gas cooler and filter; the filters are set in series and parallel. The low-pressure extraction and cooling melamine production process device of the present invention has less construction investment, low consumption, high operating flexibility, high-grade product rate can reach 95%, and the continuous operation period of the device can reach more than 4 to 6 months.

Description

technical field [0001] The invention relates to a melamine production process, in particular to an energy-saving low-pressure extraction and cooling melamine production process. Background technique [0002] Early domestic melamine production equipment generally had problems such as small scale, poor quality and high cost; in the 1980s, the domestic melamine market consumption continued to expand, and some production enterprises introduced the technology of Dutch DSM company, and 12,000 tons of melamine / year appeared Devices; In the 21st century, the domestic melamine industry has a device with an annual output of 50,000 to 80,000 tons of melamine. [0003] At present, the domestic melamine process has three mainstream processes: 30,000 tons / year low-pressure method, 50,000 tons / year low-pressure method and 50,000 tons / year high-pressure method. The main shortcoming of the low-pressure melamine process unit lies in the short operation period and high power consumption. The ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07D251/62
CPCC07D251/62Y02P20/10
Inventor 王庆锋居晓
Owner 王庆锋
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