Kaolin composite and preparation method thereof
A composite material, kaolin technology, applied in chemical instruments and methods, other chemical processes, water treatment of special compounds, etc., can solve the problems of poor PPCPs wastewater treatment effect, immature research and development of advanced oxidative degradation technology, and need to be improved, etc. The effect of reducing processing cost, improving surface-to-body ratio, and prolonging service life
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Embodiment 1
[0020] This embodiment provides a kaolin composite material, which includes CTAB intercalation modified kaolin and titanium dioxide nanoparticles (TiO2) loaded on the CTAB intercalation modified kaolin. 2 ). Specifically, the particle size of the titanium dioxide nanoparticles is 10-50 nm, and the TiO 2 Nanoparticles are loaded on the surface or in the intercalation structure of the CTAB intercalation modified kaolin, and the TiO 2 The mass ratio of nanoparticles to the CTAB intercalated modified kaolin is about 1:14.
[0021] The present embodiment also provides a method for preparing the above-mentioned kaolin composite material, which includes the following steps:
[0022] Preparation of intercalated modified kaolin: first add 10 parts by mass of kaolin raw soil to 100 volumes of powdered deionized water and mix evenly, then heat to 70°C and keep the temperature for 1 hour to obtain a suspension; add 1 mass part of cetyltrimethylammonium bromide, stirred at room temperat...
Embodiment 2
[0026] This embodiment provides a kaolin composite material, the structure of the kaolin composite material is basically the same as that of the PPCPs pollutants provided in Example 1, the main difference is that the TiO 2 The mass ratio of nanoparticles to the CTAB intercalation modified kaolin is about 1:20.
[0027] The preparation method of the above-mentioned kaolin composite material provided in this example is basically the same as that provided in Example 1, the main difference is that in the step of preparing the product in this example, the muffle furnace operates at a temperature of 3°C / min The heating rate was increased to 620°C, and the constant temperature calcination time was 12h.
Embodiment 3
[0029] This embodiment provides a kaolin composite material, the structure of the kaolin composite material is basically the same as that of the PPCPs pollutants provided in Example 1, the main difference is that the TiO 2 The particle size of the nanoparticles is 30-80nm, and the TiO 2 Nanoparticles are substantially loaded on the surface of the CTAB intercalated kaolin, and the TiO 2 The mass ratio of nanoparticles to the CTAB intercalated modified kaolin is about 1:30.
[0030] The preparation method of the above-mentioned kaolin composite material provided in this example is basically the same as the preparation method provided in Example 1, the main difference is that in the step of preparing the product in this example, the muffle furnace operates at 4°C / min The heating rate was increased to 580°C, and the constant temperature calcination time was 8h.
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