Aqueous gravure ink for tipping paper and preparation method thereof
A technology of gravure ink and tipping paper, which is applied in the field of water-based gravure ink for tipping paper and its preparation, and can solve problems such as excessive water absorption by tipping paper, great influence on cigarette smoking, and uneven dilution of smoke, etc. , to achieve the effect of loose film formation, small extensibility, and soft odor absorption
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Embodiment 1
[0049] Table 1 Formula of modified casein solution
[0050] Substance name
[0051] Add 52.9g of deionized water and casein into the reaction kettle, heat up to 65°C, add dropwise borax, sodium silicate and triethanolamine dissolved in 10g of deionized water, stir until the casein is completely dissolved, and adjust the pH to 7.5; Raise the temperature to 75°C, add dropwise the mixed monomer of N-vinylpyrrolidone, acrylonitrile and trimethylolpropane triacrylate, and drop potassium persulfate dissolved in 5g deionized water at the same time, react for 4h, add 1,2 -benzisothiazol-3-one to obtain a modified casein solution.
[0052] Table 2 water-based gravure ink formula for tipping paper
[0053] Substance name
[0054]Wetting and dispersing agent, defoamer, 15g deionized water, modified casein solution of Example 1, iron oxide yellow, iron oxide red and calcium carbonate were put into the reaction kettle in sequence, and dispersed at a high speed at a sti...
Embodiment 2
[0056] Table 3 Formula of modified casein solution
[0057] Substance name
[0058] Add 46.4g of deionized water and casein into the reaction kettle, heat up to 55°C, add dropwise borax and triethanolamine dissolved in 10g of deionized water, stir until the casein is completely dissolved, and adjust the pH to 7.9; heat up to 80°C , add dropwise the mixed monomer of N-vinylpyrrolidone, acrylonitrile and trimethylolpropane triacrylate, and dropwise add sodium persulfate dissolved in 5g deionized water at the same time, react for 4h, add 2-(4-thiazolyl ) benzimidazole and 1,2-benzisothiazol-3-one to obtain a modified casein solution.
[0059] Table 4 water-based gravure ink formula for tipping paper
[0060] Substance name
[0061] Put defoamer, modified casein solution of Example 2, iron oxide yellow, iron oxide red, iron oxide black and barium sulfate in the reaction kettle in turn, disperse at a high speed at a stirring speed of 800r / min, and then pass thr...
Embodiment 3
[0063] Table 5 Formula of modified casein solution
[0064] Substance name
[0065] Add 44.9g of deionized water and casein into the reaction kettle, heat up to 60°C, add dropwise borax and ethanolamine dissolved in 10g of deionized water, stir until the casein is completely dissolved, and adjust the pH value to 7.9; heat up to 80°C, Add dropwise the mixed monomer of N-vinylpyrrolidone, acrylonitrile and trimethylolpropane triacrylate, and dropwise add tert-butyl hydroperoxide dissolved in 5g deionized water at the same time, react for 4.5h, add 2-n-octyl Base-4-isothiazolin-3-one to obtain a modified casein solution.
[0066] Table 6 water-based gravure ink formula for tipping paper
[0067] Substance name
[0068] Drop into lubricating dispersant, defoamer, 22g deionized water, the modified casein solution of embodiment 3, iron oxide yellow, iron oxide black, calcium carbonate and talcum powder successively in the reaction kettle, with the stirring speed...
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