Hollow-structure nano tungsten oxide wire prepared through in-situ growth of graphene oxide
A nano-tungsten oxide, in-situ growth technology, applied in the field of nano-materials, can solve the problems of high conditions and high energy consumption, and achieve the effects of high purity, simple process and large production volume
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Embodiment 1
[0023] The invention provides a graphene oxide in-situ growth method for preparing hollow nano-tungsten oxide wires, which is characterized in that it is formed by mixing a certain amount of graphene oxide, a precursor compound containing tungsten, absolute ethanol, and deionized water.
[0024] In the above, the tungsten-containing precursor compound is a mixture of ammonium metatungstate and tungsten carbonyl, and the mass percentage of tungsten carbonyl in the mixture to ammonium metatungstate is 1-5%; so that graphene oxide and The tungsten precursor compounds have different molar ratios. ; Graphene oxide is graphene oxide prepared by a redox method, and the mass ratio of tungsten-containing precursor compound to graphene oxide is 1:1-6; graphene oxide is wetted with a certain amount of absolute ethanol, The mass percentage of graphene oxide is 0.1~0.5%; dispersed in a certain amount of deionized water, the mass percentage of deionized water in the wetting solution is 5~8%...
Embodiment 2
[0031] A certain amount of graphite powder was added to a solution consisting of concentrated H2SO4 (12mL), K2S2O8 (2.5g) and P2O5 (2.5g), and reacted at 80°C for 4.5 hours. After cooling to room temperature, 0.5 L of deionized water was added. and dry at room temperature. Add this pre-oxidized graphite powder to 150mL of concentrated H2SO4, keep the environment at 0°C with an ice-water bath, gradually add 15g KMnO4, and keep the temperature not exceeding 20°C, and stir at 35°C for 2 hours after the addition. Then 250 mL of deionized water was added and stirred for 2 hours. Then add 0.7 L of deionized water, then add 30 mL of 30% H2O2, dry at room temperature, and then dialyze in a dialysis bag for 1 week to remove heteroions. Finally, it was vacuum filtered and dried at room temperature to obtain graphene oxide.
[0032] Weigh 2g of graphene oxide, add 1000g of absolute ethanol, stir and mix evenly, add 60g of deionized water to mix, in the ultrasonic disperser, select 10m...
Embodiment 3
[0034]A certain amount of graphite powder was added to a solution consisting of concentrated H2SO4 (12mL), K2S2O8 (2.5g) and P2O5 (2.5g), and reacted at 80°C for 4.5 hours. After cooling to room temperature, 0.5 L of deionized water was added. and dry at room temperature. Add this pre-oxidized graphite powder to 150mL of concentrated H2SO4, keep the environment at 0°C with an ice-water bath, gradually add 15g KMnO4, and keep the temperature not exceeding 20°C, and stir at 35°C for 2 hours after the addition. Then 250 mL of deionized water was added and stirred for 2 hours. Then add 0.7 L of deionized water, then add 30 mL of 30% H2O2, dry at room temperature, and then dialyze in a dialysis bag for 1 week to remove heteroions. Finally, it was vacuum filtered and dried at room temperature to obtain graphene oxide.
[0035] Weigh 3g of graphene oxide, add 1000g of absolute ethanol, stir and mix evenly, add 700g of deionized water for mixing, in the ultrasonic disperser, select...
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