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Method and Application of Separation and Preparation of Tobacco Additives from Maillard Reaction Product of Oriented Tobacco

An additive, oriental tobacco technology, applied in the direction of tobacco, application, treatment of tobacco, etc., can solve the problems of increased roughness and dryness, unfavorable for cigarette smoking, and increase cigarette aroma, etc. Rich in gas, adding the effect of tobacco flavor

Active Publication Date: 2020-09-11
WUHAN HUANGHELOU FLAVOR & SPICES
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Although the Maillard reaction product of the oriental tobacco extract obtained through the Maillard reaction can better compensate for the aroma, but due to the lack of selective separation of the aroma components, it contains some substances that are not conducive to cigarette smoking. The smoke aroma also brings side effects such as discomfort from smoking, increased roughness and dryness

Method used

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  • Method and Application of Separation and Preparation of Tobacco Additives from Maillard Reaction Product of Oriented Tobacco

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Embodiment 1, the method and application of the preparation of tobacco additives by separating the flavor components of oriental tobacco Maillard reaction products, including the following steps:

[0026] a. Pulverize 10kg of oriental tobacco, add 100L of 50% ethanol and stir for extraction for 2 hours, the extraction temperature is 65°C; after filtering the extract, take out the filtrate and concentrate it in vacuum at 50°C to obtain oriental tobacco extract, oriental tobacco extraction The density of paste relative to water is 1.150~1.200;

[0027] B, carry out Maillard reaction with the oriental tobacco extract of gained: take by weighing 100g of oriental tobacco extract prepared in step a, 30g of glucose, 20g of proline, then it is mixed evenly, puts into conventional small reaction kettle, The temperature is controlled at 100°C, and the Maillard reaction is carried out under constant stirring for 6 hours to obtain the Maillard reaction product of oriental tobacco e...

Embodiment 2

[0030] Embodiment 2, the method and application of preparing tobacco additives by separating the flavor components of oriental tobacco Maillard reaction products, including the following steps:

[0031] a. Pulverize 10kg of oriental tobacco, add 80L of 50% ethanol and stir for extraction for 3 hours, the extraction temperature is 50°C, filter the extract, take out the filtrate and concentrate in vacuum at 50°C to obtain oriental tobacco extract, oriental tobacco extract The density of paste relative to water is 1.150~1.200;

[0032] B, carry out Maillard reaction with the oriental tobacco extract of gained: take by weighing 100g of oriental tobacco extract prepared in step a, 20g of glucose, 30g of tryptophan, then it is mixed evenly, puts into conventional small reaction kettle, The temperature is controlled at 90°C, and the Maillard reaction is carried out for 5 hours under constant stirring to obtain the Maillard reaction product of oriental tobacco extract;

[0033] C, th...

Embodiment 3

[0035] Embodiment 3, the method and application of the preparation of tobacco additives by separating the flavor components of oriental tobacco Maillard reaction products, including the following steps:

[0036]a. Crush 10kg of oriental tobacco, add 120L of ethanol with a concentration of 50% and stir for extraction for 2 hours. The extraction temperature is 70°C. After filtering the extract, take out the filtrate and concentrate it in vacuum at 50°C to obtain oriental tobacco extract. The density of the paste relative to water is 1.150-1.200, which is the oriental tobacco extract;

[0037] b. Perform Maillard reaction on the obtained oriental tobacco extract: weigh 100g of oriental tobacco extract, 30g of fructose, and 30g of alanine, then mix them evenly, put them into a conventional small reaction kettle, and control the temperature at 100°C , carrying out the Maillard reaction in constant stirring for 5 hours to obtain the Maillard reactant of oriental tobacco extract;

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Abstract

The invention provides a method for preparing a tobacco additive by separation of a fragrant ingredient of a Maillard reactant in aromatic tobacco and application. The preparation method of the tobacco additive comprises the following steps: cutting the aromatic tobacco, and then, adding ethanol for extracting, filtering and concentrating so as to obtain aromatic tobacco extract; then, adding reducing sugar and amino acid while continuously stirring to carry out Maillard reaction; adding the reactant into a molecular distillation instrument for carrying out primary distillation, and reserving primary distillate flowing out along a vacuum cavity wall; and carrying out secondary distillation so as to obtain a fragrant substance, namely the tobacco additive. By spraying the fragrant substance into shredded tobacco, the fume quality can be improved, the tobacco fragrance can be enhanced, the tobacco fume is rich, sweet, pure and mild, burrs can be restrained, impurities can be reduced, the tobacco fragrance can be enriched, and the smooth and sweet feeling of the fume can be enhanced.

Description

technical field [0001] The invention relates to the field of tobacco, in particular to a method for preparing tobacco additives by separating and preparing flavor components of oriental tobacco Maillard reaction products and the field of obtaining a novel flavor and fragrance for tobacco by application. Background technique [0002] At present, both domestic and foreign cigarette markets require cigarette products to have the attributes of "high aroma, high concentration, and low tar". As smoking and health are more and more concerned by the whole society, improving cigarette safety and developing low-tar cigarettes have become the main direction and development trend of the tobacco industry. However, while reducing cigarette tar, it often causes smoke aroma Loss and weakening of concentration, this just must make up for the flavor of cigarette by means of flavoring, thereby satisfying the smoking demand of consumers. [0003] Oriented tobacco is a type of tobacco rich in a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A24B15/24C11B9/00
CPCA24B15/24C11B9/0003
Inventor 张辉吕品陈胜
Owner WUHAN HUANGHELOU FLAVOR & SPICES
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