Method and Application of Separation and Preparation of Tobacco Additives from Maillard Reaction Product of Oriented Tobacco
An additive, oriental tobacco technology, applied in the direction of tobacco, application, treatment of tobacco, etc., can solve the problems of increased roughness and dryness, unfavorable for cigarette smoking, and increase cigarette aroma, etc. Rich in gas, adding the effect of tobacco flavor
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Embodiment 1
[0025] Embodiment 1, the method and application of the preparation of tobacco additives by separating the flavor components of oriental tobacco Maillard reaction products, including the following steps:
[0026] a. Pulverize 10kg of oriental tobacco, add 100L of 50% ethanol and stir for extraction for 2 hours, the extraction temperature is 65°C; after filtering the extract, take out the filtrate and concentrate it in vacuum at 50°C to obtain oriental tobacco extract, oriental tobacco extraction The density of paste relative to water is 1.150~1.200;
[0027] B, carry out Maillard reaction with the oriental tobacco extract of gained: take by weighing 100g of oriental tobacco extract prepared in step a, 30g of glucose, 20g of proline, then it is mixed evenly, puts into conventional small reaction kettle, The temperature is controlled at 100°C, and the Maillard reaction is carried out under constant stirring for 6 hours to obtain the Maillard reaction product of oriental tobacco e...
Embodiment 2
[0030] Embodiment 2, the method and application of preparing tobacco additives by separating the flavor components of oriental tobacco Maillard reaction products, including the following steps:
[0031] a. Pulverize 10kg of oriental tobacco, add 80L of 50% ethanol and stir for extraction for 3 hours, the extraction temperature is 50°C, filter the extract, take out the filtrate and concentrate in vacuum at 50°C to obtain oriental tobacco extract, oriental tobacco extract The density of paste relative to water is 1.150~1.200;
[0032] B, carry out Maillard reaction with the oriental tobacco extract of gained: take by weighing 100g of oriental tobacco extract prepared in step a, 20g of glucose, 30g of tryptophan, then it is mixed evenly, puts into conventional small reaction kettle, The temperature is controlled at 90°C, and the Maillard reaction is carried out for 5 hours under constant stirring to obtain the Maillard reaction product of oriental tobacco extract;
[0033] C, th...
Embodiment 3
[0035] Embodiment 3, the method and application of the preparation of tobacco additives by separating the flavor components of oriental tobacco Maillard reaction products, including the following steps:
[0036]a. Crush 10kg of oriental tobacco, add 120L of ethanol with a concentration of 50% and stir for extraction for 2 hours. The extraction temperature is 70°C. After filtering the extract, take out the filtrate and concentrate it in vacuum at 50°C to obtain oriental tobacco extract. The density of the paste relative to water is 1.150-1.200, which is the oriental tobacco extract;
[0037] b. Perform Maillard reaction on the obtained oriental tobacco extract: weigh 100g of oriental tobacco extract, 30g of fructose, and 30g of alanine, then mix them evenly, put them into a conventional small reaction kettle, and control the temperature at 100°C , carrying out the Maillard reaction in constant stirring for 5 hours to obtain the Maillard reactant of oriental tobacco extract;
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