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A device and method for continuous coating of nanoparticles by spatial atomic layer deposition

A technology of atomic layer deposition and nanoparticle, which is applied in nanotechnology, coating, gaseous chemical plating, etc., can solve the problems of not considering the isolation of precursors, the difficulty of pipeline processing, and the excessive size of the device, so as to achieve convenient process Contrastive test, convenient adjustment of experimental process, and the effect of improving efficiency

Active Publication Date: 2019-07-09
HUAZHONG UNIV OF SCI & TECH
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  • Abstract
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Problems solved by technology

[0005] (1) Only single-layer coating of nanoparticles can be achieved, and the deposition efficiency is low;
[0006] (2) The size of the device is too long, the processing of the pipeline is difficult, and the cleaning of the tube wall after the reaction is difficult;
[0007] (3) The precursor isolation problem in the coating process is not considered, and pollution will occur

Method used

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  • A device and method for continuous coating of nanoparticles by spatial atomic layer deposition
  • A device and method for continuous coating of nanoparticles by spatial atomic layer deposition
  • A device and method for continuous coating of nanoparticles by spatial atomic layer deposition

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Embodiment Construction

[0043] In order to make the object, technical solution and advantages of the present invention clearer, the present invention will be further described in detail below in conjunction with the accompanying drawings and embodiments. It should be understood that the specific embodiments described here are only used to explain the present invention, not to limit the present invention. In addition, the technical features involved in the various embodiments of the present invention described below can be combined with each other as long as they do not constitute a conflict with each other.

[0044] The basic principle of the present invention is to use multi-stage pipelines and gas flow control to make the nanoparticles move continuously in the pipeline, and then pass through the cleaning area or the precursor reaction area to realize the uniform coating of the nanoparticles. It adopts the principle of space isolation, so that The different processes of atomic layer deposition do no...

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Abstract

A nanoparticle continuous-coating device based on spatial atomic layer deposition. A first-stage pipeline unit, a second-stage pipeline unit, a third-stage pipeline unit and a fourth-stage pipeline unit which are connected sequentially. The first-stage pipeline unit is used for providing a first precursor and enabling the first precursor to be adsorbed on surfaces of nanoparticles. The third-stage pipeline unit is used for providing a second precursor and enabling the second precursor to react with the first precursor on the surfaces of the nanoparticles, so that a monomolecular thin film layer is generated on the surfaces of the nanoparticles. The second-stage and fourth-stage pipeline units are used for cleaning the nanoparticles and discharging the redundant first precursor, the redundant second precursor or reaction by-products.

Description

technical field [0001] The invention belongs to the technical field of atomic layer deposition, and in particular relates to a continuous coating device and method for atomic layer deposition of nanoparticles in space. Background technique [0002] Powder particles have a series of excellent chemical and physical properties at the microscopic level, but at the same time, they also show disadvantages such as easy agglomeration, oxidation and unstable properties. By coating the surface of the powder particles with a protective film, the above shortcomings can be effectively overcome, and the powder particles with a protective film can also be used as a new composite material with excellent performance. [0003] At present, the coating methods of powder particles mainly include solid-phase method, liquid-phase method and gas-phase method. As a special chemical vapor deposition technology, atomic layer deposition technology has excellent uniformity and reliability compared with ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C16/455C23C16/44C23C16/54B82Y40/00
CPCB82Y40/00C23C16/4417C23C16/45525C23C16/54C23C16/45551
Inventor 陈蓉巴伟明曲锴李云曹坤但威
Owner HUAZHONG UNIV OF SCI & TECH
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